12-[12-(4-Nitro-phenylamino)-dodecanoylamino]-dodecanoic acid 2,5-dioxo-pyrrolidin-1-yl ester

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Chemical Name:12-[12-(4-Nitro-phenylamino)-dodecanoylamino]-dodecanoic acid 2,5-dioxo-pyrrolidin-1-yl ester
CAS No.:125802-82-6
Molecular Formula:C₃₄H₅₄N₄O₇
Molecular Weight:630.825
Hs Code.:

Synonyms:12-[12-(4-Nitro-phenylamino)-dodecanoylamino]-dodecanoic acid 2,5-dioxo-pyrrolidin-1-yl ester

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Chemical Property of 12-[12-(4-Nitro-phenylamino)-dodecanoylamino]-dodecanoic acid 2,5-dioxo-pyrrolidin-1-yl ester

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Technology Process of 12-[12-(4-Nitro-phenylamino)-dodecanoylamino]-dodecanoic acid 2,5-dioxo-pyrrolidin-1-yl ester

There total 5 articles about 12-[12-(4-Nitro-phenylamino)-dodecanoylamino]-dodecanoic acid 2,5-dioxo-pyrrolidin-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116045-41-1
N-(4-nitrophenyl)-12-aminododecanoic acid

: 125802-82-6
12-[12-(4-Nitro-phenylamino)-dodecanoylamino]-dodecanoic acid 2,5-dioxo-pyrrolidin-1-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) RT, overnight

2: dioxane / 4 h / 50 - 60 °C

3: dicyclohexylcarbodiimide / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) RT, overnight

With dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/ja00163a005

Reference yield:

: 125802-85-9
12-(4-Nitro-phenylamino)-dodecanoic acid 2,5-dioxo-pyrrolidin-1-yl ester

: 125802-82-6
12-[12-(4-Nitro-phenylamino)-dodecanoylamino]-dodecanoic acid 2,5-dioxo-pyrrolidin-1-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dioxane / 4 h / 50 - 60 °C

2: dicyclohexylcarbodiimide / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) RT, overnight

With dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/ja00163a005

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 125802-82-6
12-[12-(4-Nitro-phenylamino)-dodecanoylamino]-dodecanoic acid 2,5-dioxo-pyrrolidin-1-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / KOH / ethanol / 24 h / Heating

2: dicyclohexylcarbodiimide / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) RT, overnight

3: dioxane / 4 h / 50 - 60 °C

4: dicyclohexylcarbodiimide / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) RT, overnight

With potassium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; ethanol;
DOI:10.1021/ja00163a005