C₂₅H₂₉BO₄

Base Information

Chemical Name:C₂₅H₂₉BO₄
CAS No.:1477517-36-4
Molecular Formula:C₂₅H₂₉BO₄
Molecular Weight:404.314
Hs Code.:

C<sub>25</sub>H<sub>29</sub>BO<sub>4</sub>

Synonyms:C₂₅H₂₉BO₄

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Chemical Property of C₂₅H₂₉BO₄

Chemical Property:

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Technology Process of C₂₅H₂₉BO₄

There total 8 articles about C₂₅H₂₉BO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1477517-35-3
C₂₀H₁₇F₃O₅S

: 73183-34-3
bis(pinacol)diborane

: 1477517-36-4
C₂₅H₂₉BO₄

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 100 ℃; for 7h; Inert atmosphere;
DOI:10.1021/ja409669r

Reference yield:

: 924-50-5
Methyl 3,3-dimethylacrylate

: 1477517-36-4
C₂₅H₂₉BO₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C

1.2: 0.5 h / -78 °C

2.1: dichloromethane / 20 h / 20 °C

2.2: 0.5 h / 20 °C

3.1: sodium dithionite dihydrate / dichloromethane; water / 1 h / 20 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

5.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

5.2: 20 °C / Inert atmosphere

6.1: potassium hydroxide / methanol / 3 h / 50 °C / Inert atmosphere

6.2: 20 °C / pH 5 - 6 / Inert atmosphere

7.1: triethylamine / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

8.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene / 1,4-dioxane / 7 h / 100 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium dithionite dihydrate; potassium acetate; sodium hydride; triethylamine; potassium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; 2.1: |Diels-Alder Cycloaddition / 2.2: |Diels-Alder Cycloaddition / 8.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ja409669r

Reference yield:

: 1477517-33-1
4-hydroxy-5-methoxy-7-methylnaphthalen-1-yl pivalate

: 1477517-36-4
C₂₅H₂₉BO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: potassium hydroxide / methanol / 3 h / 50 °C / Inert atmosphere

2.2: 20 °C / pH 5 - 6 / Inert atmosphere

3.1: triethylamine / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

4.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene / 1,4-dioxane / 7 h / 100 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; sodium hydride; triethylamine; potassium hydroxide; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; 4.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ja409669r