N-iodomethyl-N,N-dimethyl-N-(5,5-diphenyl-4-penten-1-yl)ammonium iodide

Base Information

Chemical Name:N-iodomethyl-N,N-dimethyl-N-(5,5-diphenyl-4-penten-1-yl)ammonium iodide
CAS No.:1501972-42-4
Molecular Formula:C₂₀H₂₅IN*I
Molecular Weight:533.234
Hs Code.:

Synonyms:N-iodomethyl-N,N-dimethyl-N-(5,5-diphenyl-4-penten-1-yl)ammonium iodide

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Chemical Property of N-iodomethyl-N,N-dimethyl-N-(5,5-diphenyl-4-penten-1-yl)ammonium iodide

Chemical Property:

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Technology Process of N-iodomethyl-N,N-dimethyl-N-(5,5-diphenyl-4-penten-1-yl)ammonium iodide

There total 5 articles about N-iodomethyl-N,N-dimethyl-N-(5,5-diphenyl-4-penten-1-yl)ammonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 5-(N,N-dimethyl)amino-1,1-diphenyl-1-pentene

: 75-11-6
diiodomethane

: 1501972-42-4
N-iodomethyl-N,N-dimethyl-N-(5,5-diphenyl-4-penten-1-yl)ammonium iodide

Guidance literature:: In acetonitrile; at 20 ℃; for 24h; Darkness;
DOI:10.3390/molecules21040381

Reference yield:

: 114736-31-1
5-bromo-1,1-diphenylpentan-1-ol

: 1501972-42-4
N-iodomethyl-N,N-dimethyl-N-(5,5-diphenyl-4-penten-1-yl)ammonium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / benzene / 6 h / Reflux

2: water; tetrahydrofuran / 24 h / 20 °C

3: acetonitrile / 20 h

With toluene-4-sulfonic acid; In tetrahydrofuran; water; acetonitrile; benzene;

Reference yield:

: 100-58-3
phenylmagnesium bromide

: 1501972-42-4
N-iodomethyl-N,N-dimethyl-N-(5,5-diphenyl-4-penten-1-yl)ammonium iodide

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether / 0.25 h / 0 °C / Inert atmosphere

2: toluene-4-sulfonic acid / benzene / 6 h / Reflux

3: water; tetrahydrofuran / 24 h / 20 °C

4: acetonitrile / 20 h

With toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; water; acetonitrile; benzene;