6,7-dichloro-1,4-di-N-oxide-3-methylquinoxaline-2-carboxylic acid 2-benzylamide

Base Information

Chemical Name:6,7-dichloro-1,4-di-N-oxide-3-methylquinoxaline-2-carboxylic acid 2-benzylamide
CAS No.:1228550-65-9
Molecular Formula:C₁₇H₁₃Cl₂N₃O₃
Molecular Weight:378.215
Hs Code.:

Synonyms:6,7-dichloro-1,4-di-N-oxide-3-methylquinoxaline-2-carboxylic acid 2-benzylamide

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Chemical Property of 6,7-dichloro-1,4-di-N-oxide-3-methylquinoxaline-2-carboxylic acid 2-benzylamide

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Technology Process of 6,7-dichloro-1,4-di-N-oxide-3-methylquinoxaline-2-carboxylic acid 2-benzylamide

There total 3 articles about 6,7-dichloro-1,4-di-N-oxide-3-methylquinoxaline-2-carboxylic acid 2-benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 882-36-0
N-benzyl-3-oxobutanamide

: 4701-01-3
5,6-dichlorobenzofuroxan

: 1228550-65-9
6,7-dichloro-1,4-di-N-oxide-3-methylquinoxaline-2-carboxylic acid 2-benzylamide

Guidance literature:: With ethanolamine; calcium chloride; In methanol; at 20 ℃;
DOI:10.1016/j.bmc.2010.02.024

Reference yield:

: 6641-64-1
4,5-dichloro-2-nitroaniline

: 1228550-65-9
6,7-dichloro-1,4-di-N-oxide-3-methylquinoxaline-2-carboxylic acid 2-benzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hypochlorite / N,N-dimethyl-formamide / 20 °C

2: ethanolamine; calcium chloride / methanol

With sodium hypochlorite; ethanolamine; calcium chloride; In methanol; N,N-dimethyl-formamide; 2: Beirut reaction;
DOI:10.3390/molecules16097893

Reference yield:

: 100-46-9
benzylamine

: 1228550-65-9
6,7-dichloro-1,4-di-N-oxide-3-methylquinoxaline-2-carboxylic acid 2-benzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 0 °C / Inert atmosphere

2: ethanolamine; calcium chloride / methanol

With ethanolamine; calcium chloride; In methanol; 2: Beirut reaction;
DOI:10.3390/molecules16097893