heptaacetyl-O-4-methoxybenzyl-6-O-(β-D-glucopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:heptaacetyl-O-4-methoxybenzyl-6-O-(β-D-glucopyranosyl)-β-D-glucopyranoside
CAS No.:888945-74-2
Molecular Formula:C₃₄H₄₄O₁₉
Molecular Weight:756.712
Hs Code.:

Synonyms:heptaacetyl-O-4-methoxybenzyl-6-O-(β-D-glucopyranosyl)-β-D-glucopyranoside

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Chemical Property of heptaacetyl-O-4-methoxybenzyl-6-O-(β-D-glucopyranosyl)-β-D-glucopyranoside

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Technology Process of heptaacetyl-O-4-methoxybenzyl-6-O-(β-D-glucopyranosyl)-β-D-glucopyranoside

There total 3 articles about heptaacetyl-O-4-methoxybenzyl-6-O-(β-D-glucopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 105-13-5
4-Methoxybenzyl alcohol

: 888945-73-1
2,4,6-tri-O-acetyl-6-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-β-D-glucopyranosyl trichloroacetimidate

: 888945-74-2
heptaacetyl-O-4-methoxybenzyl-6-O-(β-D-glucopyranosyl)-β-D-glucopyranoside

Guidance literature:: boron trifluoride diethyl etherate; In dichloromethane; at -50 - 20 ℃; for 3.25h;

Reference yield:

: 105-13-5
4-Methoxybenzyl alcohol

: 909100-37-4
O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranosyl)trichloroacetimidate

: 888945-74-2
heptaacetyl-O-4-methoxybenzyl-6-O-(β-D-glucopyranosyl)-β-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -50 - 25 ℃;
DOI:10.1016/j.bmcl.2004.12.071

Reference yield:

: 61091-11-0
Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-2-((S)-cyano-phenyl-methoxy)-6-((2R,3R,4S,5R,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-3-yl ester

: 888945-74-2
heptaacetyl-O-4-methoxybenzyl-6-O-(β-D-glucopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / Pd(OH)2/C / toluene; acetone / 3 h / 25 °C / 750.06 Torr

2: NaH / CH₂Cl₂ / 0.25 h / 25 °C

3: BF₃*Et₂O / CH₂Cl₂ / -50 - 25 °C

With palladium dihydroxide; boron trifluoride diethyl etherate; sodium hydride; In dichloromethane; acetone; toluene;
DOI:10.1016/j.bmcl.2004.12.071