methoxy-6, phenyl-1, dihydro-3,4 naphtalene

Base Information

Chemical Name:methoxy-6, phenyl-1, dihydro-3,4 naphtalene
CAS No.:2844-82-8
Molecular Formula:C₁₇H₁₆O
Molecular Weight:236.313
Hs Code.:

Synonyms:methoxy-6, phenyl-1, dihydro-3,4 naphtalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methoxy-6, phenyl-1, dihydro-3,4 naphtalene

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Technology Process of methoxy-6, phenyl-1, dihydro-3,4 naphtalene

There total 10 articles about methoxy-6, phenyl-1, dihydro-3,4 naphtalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 3262-89-3
triphenylboroxine

: 1078-19-9
6-methoxy-3,4-dihydro-1(2H)-naphthalenone

: 2844-82-8
methoxy-6, phenyl-1, dihydro-3,4 naphtalene

Guidance literature:: With tetrakis(triphenylphosphine)nickel⁽⁰⁾; water; 1,2-bis-(dicyclohexylphosphino)ethane; In diethylene glycol dimethyl ether; at 120 ℃; for 24h; Glovebox; Schlenk technique; Inert atmosphere;
DOI:10.1021/jacs.7b02742

Reference yield:

: 100-58-3
phenylmagnesium bromide

: 1078-19-9
6-methoxy-3,4-dihydro-1(2H)-naphthalenone

: 2844-82-8
methoxy-6, phenyl-1, dihydro-3,4 naphtalene

Guidance literature:: With sodium chloride; sulfuric acid; ammonium chloride; sodium hydrogencarbonate; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; diethyl ether; acetic acid; ethyl acetate;

Reference yield:

: 7664-93-9
sulfuric acid

: 100-58-3
phenylmagnesium bromide

: 1078-19-9
6-methoxy-3,4-dihydro-1(2H)-naphthalenone

: 2844-82-8
methoxy-6, phenyl-1, dihydro-3,4 naphtalene

Guidance literature:: phenylmagnesium bromide; 6-methoxy-3,4-dihydro-1(2H)-naphthalenone; In diethyl ether; at 20 ℃; for 4h; Heating / reflux;

sulfuric acid; In acetic acid; at 20 ℃; for 1.5h;