tert-butyl 3-nitrocinnamic acid

Base Information

Chemical Name:tert-butyl 3-nitrocinnamic acid
CAS No.:942232-49-7
Molecular Formula:C₁₃H₁₅NO₄
Molecular Weight:249.266
Hs Code.:

Synonyms:tert-butyl 3-nitrocinnamic acid

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Chemical Property of tert-butyl 3-nitrocinnamic acid

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Technology Process of tert-butyl 3-nitrocinnamic acid

There total 3 articles about tert-butyl 3-nitrocinnamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 645-00-1
m-iodonitrobenzene

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 942232-49-7
tert-butyl 3-nitrocinnamic acid

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 120 ℃; for 3h; Schlenk technique; Green chemistry;
DOI:10.1039/c7nj04361a

Reference yield: 60.0%

: 5765-65-1
4-(benzoyloxy)morpholine

: 645-00-1
m-iodonitrobenzene

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 942232-49-7
tert-butyl 3-nitrocinnamic acid

: C₁₇H₂₂N₂O₅

Guidance literature:: With bis(η3-allyl-μ-chloropalladium(II)); C₁₃H₂₀; caesium carbonate; ruphos; In 1,4-dioxane; toluene; at 100 ℃; for 24h;
DOI:10.1038/s41557-018-0074-z