(1'R,4S)-4-(1',5'-dimethylhex-4'-en-1'-yl)cyclohexa-1,5-diene-1-carboxylic acid

Base Information

• Chemical Name: (1'R,4S)-4-(1',5'-dimethylhex-4'-en-1'-yl)cyclohexa-1,5-diene-1-carboxylic acid
• CAS No.: 1253784-47-2
• Molecular Formula: C₁₅H₂₂O₂
• Molecular Weight: 234.338

Synonyms:(1'R,4S)-4-(1',5'-dimethylhex-4'-en-1'-yl)cyclohexa-1,5-diene-1-carboxylic acid

Chemical Property of (1'R,4S)-4-(1',5'-dimethylhex-4'-en-1'-yl)cyclohexa-1,5-diene-1-carboxylic acid

Chemical Property:

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Technology Process of (1'R,4S)-4-(1',5'-dimethylhex-4'-en-1'-yl)cyclohexa-1,5-diene-1-carboxylic acid

There total 1 articles about (1'R,4S)-4-(1',5'-dimethylhex-4'-en-1'-yl)cyclohexa-1,5-diene-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon monoxide (201230-82-2) + C15H21F3O3S → (1'R,4R)-4-(1',5'-dimethylhex-4'-en-1'-yl)cyclohexa-1,5-diene-1-carboxylic acid (1253784-46-1) + (1'R,4S)-4-(1',5'-dimethylhex-4'-en-1'-yl)cyclohexa-1,5-diene-1-carboxylic acid (1253784-47-2)

Guidance literature:

carbon monoxide; C₁₅H₂₁F₃O₃S; With potassium acetate; palladium diacetate; triphenylphosphine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

With water; sodium hydroxide; In N,N-dimethyl-formamide;

With hydrogenchloride; In water;

DOI:10.1021/jo101088h

Reference yield: 70.0%

(1'R,4S)-4-(1',5'-dimethylhex-4'-en-1'-yl)cyclohexa-1,5-diene-1-carboxylic acid (1253784-47-2) + trans-4-[(1E,3E)-1,5-dimethylhexa-1,3,5-trien-1-yl]cyclo-hexanecarboxylic acid (1253784-40-5) → C30H44O4 + C30H44O4 (1254104-82-9)

Guidance literature:

With (2-bromophenyl)boronic acid; In dichloromethane; at 50 ℃; for 72h; optical yield given as %de; diastereoselective reaction; Inert atmosphere; Darkness;

DOI:10.1021/jo101088h

upstream raw materials:

carbon monoxide

Downstream raw materials:

C₃₀H₄₄O₄

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