tert-Butyl-{4-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-2-methoxy-phenoxy}-dimethyl-silane

Base Information

• Chemical Name: tert-Butyl-{4-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-2-methoxy-phenoxy}-dimethyl-silane
• CAS No.: 175360-95-9
• Molecular Formula: C₂₃H₃₂O₄Si
• Molecular Weight: 400.59

Synonyms:tert-Butyl-{4-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-2-methoxy-phenoxy}-dimethyl-silane

Chemical Property of tert-Butyl-{4-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-2-methoxy-phenoxy}-dimethyl-silane

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Technology Process of tert-Butyl-{4-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-2-methoxy-phenoxy}-dimethyl-silane

There total 1 articles about tert-Butyl-{4-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-2-methoxy-phenoxy}-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

(E)-4-(3,4-dimethoxystyryl)-2-methoxyphenol (54083-20-4) + tert-butyldimethylsilyl chloride (18162-48-6) → tert-Butyl-{4-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-2-methoxy-phenoxy}-dimethyl-silane (175360-95-9)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; for 24h; Ambient temperature;

DOI:10.1139/v96-030

Reference yield: 19.0%

tert-Butyl-{4-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-2-methoxy-phenoxy}-dimethyl-silane (175360-95-9) → 6-(tert-butyldimethylsiloxy)-2,3,5-trimethoxyphenanthrene (175360-98-2) + trans-1,2-bis(3,4-dimethoxyphenyl)-cis,trans-3,4-bis(4-tert-butyldimethylsiloxy-3-methoxyphenyl)-cyclobutane + cis-1,3-bis(3,4-dimethoxyphenyl)-trans,trans-2,4-bis(4-tert-butyldimethylsiloxy-3-methoxyphenyl)-cyclobutane + tert-Butyl-{4-[(Z)-2-(3,4-dimethoxy-phenyl)-vinyl]-2-methoxy-phenoxy}-dimethyl-silane

Guidance literature:

With oxygen; In tetrahydrofuran; at 27 ℃; for 12h; Further byproducts given; Irradiation;

DOI:10.1139/v96-030

Reference yield: 11.0%

tert-Butyl-{4-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-2-methoxy-phenoxy}-dimethyl-silane (175360-95-9) → 6-(tert-butyldimethylsiloxy)-2,3,5-trimethoxyphenanthrene (175360-98-2) + 3-(tert-butyldimethylsiloxy)-2,6,7-trimethoxyphenanthrene (175361-00-9) + 3-(tert-butyldimethylsiloxy)-2,5,6-trimethoxyphenanthrene (175360-99-3) + 1-ethoxy-1-(4-(tert-butyldimethylsiloxy)-3-methoxyphenyl)-2-(3,4-dimethoxyphenyl)ethane

Guidance literature:

With oxygen; In ethanol; at 20 ℃; for 1h; Further byproducts given; Irradiation;

DOI:10.1139/v96-030

upstream raw materials:

(E)-4-(3,4-dimethoxystyryl)-2-methoxyphenol

tert-butyldimethylsilyl chloride

Downstream raw materials:

6-(tert-butyldimethylsiloxy)-2,3,5-trimethoxyphenanthrene

3-(tert-butyldimethylsiloxy)-2,6,7-trimethoxyphenanthrene

3-(tert-butyldimethylsiloxy)-2,5,6-trimethoxyphenanthrene

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