2-[[4-[(dimethylamino)carbonyl]phenyl]thio]-3-nitrobenzeneacetic acid methyl ester

Base Information

Chemical Name:2-[[4-[(dimethylamino)carbonyl]phenyl]thio]-3-nitrobenzeneacetic acid methyl ester
CAS No.:627488-02-2
Molecular Formula:C₁₈H₁₈N₂O₅S
Molecular Weight:374.417
Hs Code.:

Synonyms:2-[[4-[(dimethylamino)carbonyl]phenyl]thio]-3-nitrobenzeneacetic acid methyl ester

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Chemical Property of 2-[[4-[(dimethylamino)carbonyl]phenyl]thio]-3-nitrobenzeneacetic acid methyl ester

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Technology Process of 2-[[4-[(dimethylamino)carbonyl]phenyl]thio]-3-nitrobenzeneacetic acid methyl ester

There total 4 articles about 2-[[4-[(dimethylamino)carbonyl]phenyl]thio]-3-nitrobenzeneacetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(4'-acetoxymethyl-2'-nitrophenylthio)benzoic acid chloride

: 506-59-2
N,N-dimethylammonium chloride

: 627488-02-2
2-[[4-[(dimethylamino)carbonyl]phenyl]thio]-3-nitrobenzeneacetic acid methyl ester

Guidance literature:: With potassium carbonate; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jm0400808

Reference yield:

: 627487-47-2
4-[(2-carboxyphenyl)thio]-3-nitrobenzeneacetic acid α-methyl ester

: 627488-02-2
2-[[4-[(dimethylamino)carbonyl]phenyl]thio]-3-nitrobenzeneacetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 70 °C

2: K₂CO₃ / tetrahydrofuran / 20 °C

With thionyl chloride; potassium carbonate; In tetrahydrofuran;
DOI:10.1021/jm0400808

Reference yield:

: 627490-22-6
methyl 4-bromo-3-nitrophenylacetate

: 627488-02-2
2-[[4-[(dimethylamino)carbonyl]phenyl]thio]-3-nitrobenzeneacetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / Cu; K₂CO₃ / dimethylformamide / 65 °C

2: SOCl₂ / 70 °C

3: K₂CO₃ / tetrahydrofuran / 20 °C

With thionyl chloride; copper; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm0400808