3-Methoxy-4-(2-nitroethenyl)phenol

Base Information

Chemical Name:3-Methoxy-4-(2-nitroethenyl)phenol
CAS No.:4230-92-6
Molecular Formula:C₉H₉NO₄
Molecular Weight:195.175
Hs Code.:2909500000
DSSTox Substance ID:DTXSID001295492
Mol file:4230-92-6.mol

Synonyms:3-methoxy-4-(2-nitroethenyl)phenol;DTXSID001295492;4230-92-6

Suppliers and Price of 3-Methoxy-4-(2-nitroethenyl)phenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-HYDROXY-2-METHOXY-BETA-NITROSTYRENE 95.00%
5MG
$ 496.00

Total 2 raw suppliers

Chemical Property of 3-Methoxy-4-(2-nitroethenyl)phenol

Chemical Property:

PSA：75.28000
LogP:2.17140
XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:195.05315777
Heavy Atom Count:14
Complexity:223

Purity/Quality:

97% ^*data from raw suppliers

4-HYDROXY-2-METHOXY-BETA-NITROSTYRENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=CC(=C1)O)C=C[N+](=O)[O-]

Technology Process of 3-Methoxy-4-(2-nitroethenyl)phenol

There total 2 articles about 3-Methoxy-4-(2-nitroethenyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 75-52-5
nitromethane

: 18278-34-7
4-hydroxy-2-methoxybenzaldehyde

: 4230-92-6
3-Methoxy-4-(2nitrovinyl)phenol

Guidance literature:: With ammonium acetate; acetic acid; In ethanol; for 1h; Heating;
DOI:10.1016/0008-6215(86)85043-1

Reference yield:

: 150-19-6
O-methylresorcine

: 4230-92-6
3-Methoxy-4-(2nitrovinyl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1: 11 percent / 15percent KOH / CHCl₃ / 3 h / Heating

2: 56 percent / ammonium acetate, acetic acid / ethanol / 1 h / Heating

With ammonium acetate; potassium hydroxide; acetic acid; In ethanol; chloroform;
DOI:10.1016/0008-6215(86)85043-1