[1-(4-Methoxy-phenyl)-1-(4-trifluoromethyl-phenyl)-meth-(Z)-ylidene]-hydrazine

Base Information

Chemical Name:[1-(4-Methoxy-phenyl)-1-(4-trifluoromethyl-phenyl)-meth-(Z)-ylidene]-hydrazine
CAS No.:41831-09-8
Molecular Formula:C₁₅H₁₃F₃N₂O
Molecular Weight:294.276
Hs Code.:

Synonyms:[1-(4-Methoxy-phenyl)-1-(4-trifluoromethyl-phenyl)-meth-(Z)-ylidene]-hydrazine

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Chemical Property of [1-(4-Methoxy-phenyl)-1-(4-trifluoromethyl-phenyl)-meth-(Z)-ylidene]-hydrazine

Chemical Property:

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Technology Process of [1-(4-Methoxy-phenyl)-1-(4-trifluoromethyl-phenyl)-meth-(Z)-ylidene]-hydrazine

There total 5 articles about [1-(4-Methoxy-phenyl)-1-(4-trifluoromethyl-phenyl)-meth-(Z)-ylidene]-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6185-76-8
(4-methoxyphenyl)(4-(trifluoromethyl)phenyl)methanone

: 41831-09-8
[1-(4-Methoxy-phenyl)-1-(4-trifluoromethyl-phenyl)-meth-(Z)-ylidene]-hydrazine

Guidance literature:: With hydrazine hydrate; acetic acid; In ethanol; for 12h; Reflux; Schlenk technique;
DOI:10.1021/jacs.0c04725

Reference yield:

: 87901-71-1
α-(4-methoxyphenyl)(4-trifluoromethyl)benzyl alcohol

: 41831-09-8
[1-(4-Methoxy-phenyl)-1-(4-trifluoromethyl-phenyl)-meth-(Z)-ylidene]-hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 3 h / 20 °C / Schlenk technique

2: hydrazine hydrate; acetic acid / ethanol / 12 h / Schlenk technique; Reflux

With hydrazine hydrate; acetic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In ethanol; dimethyl sulfoxide;
DOI:10.1002/anie.202109447

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 41831-09-8
[1-(4-Methoxy-phenyl)-1-(4-trifluoromethyl-phenyl)-meth-(Z)-ylidene]-hydrazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium / tetrahydrofuran; ethylene dibromide / 2 h / Schlenk technique; Inert atmosphere; Reflux

1.2: 1 h / 0 °C / Schlenk technique; Inert atmosphere

2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 3 h / 20 °C / Schlenk technique

3.1: hydrazine hydrate; acetic acid / ethanol / 12 h / Schlenk technique; Reflux

With hydrazine hydrate; magnesium; acetic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; ethanol; dimethyl sulfoxide; ethylene dibromide;
DOI:10.1002/anie.202109447