1-(4-Methoxy-benzenesulfonyl)-2-((E)-tridec-8-enyl)-4-trityl-piperazine

Base Information

Chemical Name:1-(4-Methoxy-benzenesulfonyl)-2-((E)-tridec-8-enyl)-4-trityl-piperazine
CAS No.:426820-03-3
Molecular Formula:C₄₃H₅₄N₂O₃S
Molecular Weight:678.979
Hs Code.:

Synonyms:1-(4-Methoxy-benzenesulfonyl)-2-((E)-tridec-8-enyl)-4-trityl-piperazine

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Chemical Property of 1-(4-Methoxy-benzenesulfonyl)-2-((E)-tridec-8-enyl)-4-trityl-piperazine

Chemical Property:

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Technology Process of 1-(4-Methoxy-benzenesulfonyl)-2-((E)-tridec-8-enyl)-4-trityl-piperazine

There total 9 articles about 1-(4-Methoxy-benzenesulfonyl)-2-((E)-tridec-8-enyl)-4-trityl-piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16695-32-2
tetrahydropyranyl ether of 7-dodecyn-1-ol

: 426820-03-3
1-(4-Methoxy-benzenesulfonyl)-2-((E)-tridec-8-enyl)-4-trityl-piperazine

Guidance literature:: Multi-step reaction with 7 steps

1: 72 percent / Na; ammonia / diethyl ether

2: 91 percent / hydrogen chloride / methanol / 4 °C

3: 47 percent / PBr₃; pyridine / benzene / 20 °C

4: 76 percent / NaNH₂ / liquid ammonia; diethyl ether

5: 77 percent / Na; n-BuOH

6: triethylamine / CH₂Cl₂ / -13 °C

7: triethylamine / CH₂Cl₂ / 3 h / 20 °C

With pyridine; hydrogenchloride; ammonia; sodium; phosphorus tribromide; sodium amide; triethylamine; butan-1-ol; In methanol; diethyl ether; dichloromethane; ammonia; benzene; 1: Birch reduction;
DOI:10.1016/S0223-5234(01)01274-0

Reference yield:

: 55305-37-8
(7E)-1-(tetrahydropyran-2'-yloxy)-7-dodecene

: 426820-03-3
1-(4-Methoxy-benzenesulfonyl)-2-((E)-tridec-8-enyl)-4-trityl-piperazine

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / hydrogen chloride / methanol / 4 °C

2: 47 percent / PBr₃; pyridine / benzene / 20 °C

3: 76 percent / NaNH₂ / liquid ammonia; diethyl ether

4: 77 percent / Na; n-BuOH

5: triethylamine / CH₂Cl₂ / -13 °C

6: triethylamine / CH₂Cl₂ / 3 h / 20 °C

With pyridine; hydrogenchloride; sodium; phosphorus tribromide; sodium amide; triethylamine; butan-1-ol; In methanol; diethyl ether; dichloromethane; ammonia; benzene;
DOI:10.1016/S0223-5234(01)01274-0

Reference yield:

: 53963-10-3
2-[(6-bromohexyl)oxy]tetrahydro-2H-pyran

: 426820-03-3
1-(4-Methoxy-benzenesulfonyl)-2-((E)-tridec-8-enyl)-4-trityl-piperazine

Guidance literature:: Multi-step reaction with 8 steps

1: 85 percent / lithium amide / liquid ammonia; tetrahydrofuran

2: 72 percent / Na; ammonia / diethyl ether

3: 91 percent / hydrogen chloride / methanol / 4 °C

4: 47 percent / PBr₃; pyridine / benzene / 20 °C

5: 76 percent / NaNH₂ / liquid ammonia; diethyl ether

6: 77 percent / Na; n-BuOH

7: triethylamine / CH₂Cl₂ / -13 °C

8: triethylamine / CH₂Cl₂ / 3 h / 20 °C

With pyridine; hydrogenchloride; lithium amide; ammonia; sodium; phosphorus tribromide; sodium amide; triethylamine; butan-1-ol; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; ammonia; benzene; 2: Birch reduction;
DOI:10.1016/S0223-5234(01)01274-0