3,3-dimethyl-1-(5-carboxypentyl)-2-(4-anilidovinyl)-3H-indol-1-ium-5-sulfonate

Base Information

• Chemical Name: 3,3-dimethyl-1-(5-carboxypentyl)-2-(4-anilidovinyl)-3H-indol-1-ium-5-sulfonate
• CAS No.: 1251915-33-9
• Molecular Formula: C₂₆H₃₀N₂O₆S
• Molecular Weight: 498.6
• Mol file: 1251915-33-9.mol

Synonyms:3,3-dimethyl-1-(5-carboxypentyl)-2-(4-anilidovinyl)-3H-indol-1-ium-5-sulfonate

Chemical Property of 3,3-dimethyl-1-(5-carboxypentyl)-2-(4-anilidovinyl)-3H-indol-1-ium-5-sulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,3-dimethyl-1-(5-carboxypentyl)-2-(4-anilidovinyl)-3H-indol-1-ium-5-sulfonate

There total 5 articles about 3,3-dimethyl-1-(5-carboxypentyl)-2-(4-anilidovinyl)-3H-indol-1-ium-5-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(5-carboxypentyl)-2,3,3-trimethyl-3H-indolium-5-sulfonate (146368-08-3) + acetic anhydride (108-24-7) + N,N'-diphenylformamidine (864131-95-3) → 3,3-dimethyl-1-(5-carboxypentyl)-2-(4-anilidovinyl)-3H-indol-1-ium-5-sulfonate (1251915-33-9)

Guidance literature:

With acetic acid; at 120 ℃; for 1h;

Reference yield:

3-methyl-butan-2-one (563-80-4) → 3,3-dimethyl-1-(5-carboxypentyl)-2-(4-anilidovinyl)-3H-indol-1-ium-5-sulfonate (1251915-33-9)

Guidance literature:

Multi-step reaction with 3 steps

2.1: potassium hydroxide / isopropyl alcohol

2.2: 10 h / 120 °C / Inert atmosphere

3.1: acetic acid / 1 h / 120 °C

With acetic acid; potassium hydroxide; In isopropyl alcohol; 1.1: |Fischer Indole Synthesis;

Reference yield:

2,3,3-trimethylindole-5-sulfonic acid (132557-72-3) → 3,3-dimethyl-1-(5-carboxypentyl)-2-(4-anilidovinyl)-3H-indol-1-ium-5-sulfonate (1251915-33-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium hydroxide / isopropyl alcohol

1.2: 10 h / 120 °C / Inert atmosphere

2.1: acetic acid / 1 h / 120 °C

With acetic acid; potassium hydroxide; In isopropyl alcohol;

upstream raw materials:

2,3,3-trimethylindole-5-sulfonic acid

3-methyl-butan-2-one

4-hydrazino-benzenesulfonic acid

6-bromohexanoic acid