1-(1-methylethyl)-4-{[4-(tetrahydro-2H-pyran-4-yloxy)phenyl]carbonyl}piperazine hydrochloride

Base Information

Chemical Name:1-(1-methylethyl)-4-{[4-(tetrahydro-2H-pyran-4-yloxy)phenyl]carbonyl}piperazine hydrochloride
CAS No.:1125474-24-9
Molecular Formula:C₁₉H₂₈N₂O₃*ClH
Molecular Weight:368.904
Hs Code.:

Synonyms:1-(1-methylethyl)-4-{[4-(tetrahydro-2H-pyran-4-yloxy)phenyl]carbonyl}piperazine hydrochloride

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Chemical Property of 1-(1-methylethyl)-4-{[4-(tetrahydro-2H-pyran-4-yloxy)phenyl]carbonyl}piperazine hydrochloride

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Technology Process of 1-(1-methylethyl)-4-{[4-(tetrahydro-2H-pyran-4-yloxy)phenyl]carbonyl}piperazine hydrochloride

There total 4 articles about 1-(1-methylethyl)-4-{[4-(tetrahydro-2H-pyran-4-yloxy)phenyl]carbonyl}piperazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4318-42-7
1-(1-methylethyl)piperazine

: 851048-51-6
4-(3,4,5,6-tetrahydro-2H-pyran-4-yloxy)benzoic acid

: 1125474-24-9
1-(1-methylethyl)-4-{[4-(tetrahydro-2H-pyran-4-yloxy)phenyl]carbonyl}piperazine hydrochloride

Guidance literature:: 1-(1-methylethyl)piperazine; 4-(3,4,5,6-tetrahydro-2H-pyran-4-yloxy)benzoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h;

With hydrogenchloride; In diethyl ether; dichloromethane; Product distribution / selectivity;

Reference yield:

: 4318-42-7
1-(1-methylethyl)piperazine

: 892501-93-8
4-(tetrahydro-2H-pyran-4-yloxy)benzoyl chloride

: 1125474-24-9
1-(1-methylethyl)-4-{[4-(tetrahydro-2H-pyran-4-yloxy)phenyl]carbonyl}piperazine hydrochloride

Guidance literature:: 1-(1-methylethyl)piperazine; 4-(tetrahydro-2H-pyran-4-yloxy)benzoyl chloride; In dichloromethane; at 20 ℃; for 0.5h;

With hydrogenchloride; In 1,4-dioxane; dichloromethane; Product distribution / selectivity;