4-(TETRAHYDROPYRAN-4-YLOXY)BENZOIC ACID

Base Information

• Chemical Name: 4-(TETRAHYDROPYRAN-4-YLOXY)BENZOIC ACID
• CAS No.: 851048-51-6
• Molecular Formula: C12H14 O4
• Molecular Weight: 222.241
• Hs Code.: 2932999099
• Mol file: 851048-51-6.mol

Synonyms:4-(Tetrahydropyran-4-yloxy)benzoicacid; 4-[(Tetrahydro-2H-pyran-4-yl)oxy]benzoic acid

Chemical Property of 4-(TETRAHYDROPYRAN-4-YLOXY)BENZOIC ACID

Chemical Property:

• Melting Point: 185 °C
• PSA: 55.76000
• LogP: 1.94260
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-[(Tetrahydro-2H-pyran-4-yl)oxy]benzoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 41
• Safety Statements: 26-39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(TETRAHYDROPYRAN-4-YLOXY)BENZOIC ACID

There total 5 articles about 4-(TETRAHYDROPYRAN-4-YLOXY)BENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 4-((tetrahydro-2H-pyran-4-yl)oxy)benzoate (1125474-25-0) → 4-(3,4,5,6-tetrahydro-2H-pyran-4-yloxy)benzoic acid (851048-51-6) + 4-hydroxy-benzoic acid (99-96-7)

Guidance literature:

methyl 4-((tetrahydro-2H-pyran-4-yl)oxy)benzoate; With methanol; sodium hydroxide; water; at 20 ℃; for 4h; Heating / reflux;

With hydrogenchloride; water; pH=2; Product distribution / selectivity;

Reference yield:

ethyl 4-(tetrahydro-2H-pyran-4-yloxy)benzoate (851048-50-5) → 4-(3,4,5,6-tetrahydro-2H-pyran-4-yloxy)benzoic acid (851048-51-6)

Guidance literature:

With sodium hydroxide; water; In ethanol; at 60 ℃; for 5h;

Reference yield:

methyl 4-((tetrahydro-2H-pyran-4-yl)oxy)benzoate (1125474-25-0) → 4-(3,4,5,6-tetrahydro-2H-pyran-4-yloxy)benzoic acid (851048-51-6)

Guidance literature:

methyl 4-((tetrahydro-2H-pyran-4-yl)oxy)benzoate; With water; sodium hydroxide; In toluene; at 80 ℃;

With hydrogenchloride; pH=1;

upstream raw materials:

ethyl 4-(tetrahydro-2H-pyran-4-yloxy)benzoate

methyl 4-((tetrahydro-2H-pyran-4-yl)oxy)benzoate

methyl 4-hydroxylbenzoate

Tetrahydro-pyran-4-ol

Downstream raw materials:

4-(tetrahydro-2H-pyran-4-yloxy)benzoyl chloride

1-(1-methylethyl)-4-{[4-(tetrahydro-2H-pyran-4-yloxy)phenyl]carbonyl}piperazine hydrochloride

(4-isopropylpiperazin-1-yl)(4-((tetrahydro-2H-pyran-4-yl)oxy)phenyl)methanone

N-(2-methoxyethyl)-4-methyl-2-({1-[4-(3,4,5,6-tetrahydro-2H-pyran-4-yloxy)benzoyl]piperidin-4-yl}methyl)-2H-indazole-5-carboxamide

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