dec-9-enoic acid (3-{[4-(2-allyl-piperidin-1-yl)-butyl]-benzyl-amino}-propyl)-amide

Base Information

Chemical Name:dec-9-enoic acid (3-{[4-(2-allyl-piperidin-1-yl)-butyl]-benzyl-amino}-propyl)-amide
CAS No.:934807-99-5
Molecular Formula:C₃₂H₅₃N₃O
Molecular Weight:495.792
Hs Code.:

Synonyms:dec-9-enoic acid (3-{[4-(2-allyl-piperidin-1-yl)-butyl]-benzyl-amino}-propyl)-amide

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Chemical Property of dec-9-enoic acid (3-{[4-(2-allyl-piperidin-1-yl)-butyl]-benzyl-amino}-propyl)-amide

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Technology Process of dec-9-enoic acid (3-{[4-(2-allyl-piperidin-1-yl)-butyl]-benzyl-amino}-propyl)-amide

There total 5 articles about dec-9-enoic acid (3-{[4-(2-allyl-piperidin-1-yl)-butyl]-benzyl-amino}-propyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 934808-00-1
N¹-[4-((S)-2-allyl-piperidin-1-yl)-butyl]-N¹-benzyl-propane-1,3-diamine

: 116902-88-6
9-decenoic acid chloride

: 934807-99-5
dec-9-enoic acid (3-{[4-(2-allyl-piperidin-1-yl)-butyl]-benzyl-amino}-propyl)-amide

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1016/j.tet.2007.01.068

Reference yield:

: 934808-02-3
4-(2-allyl-piperidin-1-yl)-4-oxo-butyric acid

: 934807-99-5
dec-9-enoic acid (3-{[4-(2-allyl-piperidin-1-yl)-butyl]-benzyl-amino}-propyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / triethylamine; DMAP; benzoic anhydride / CH₂Cl₂ / 25 h / 20 °C

2: lithium aluminum hydride / 25 °C

3: 276 mg / triethylamine / CH₂Cl₂ / 2 h / 0 °C

With dmap; lithium aluminium tetrahydride; benzoic acid anhydride; triethylamine; In dichloromethane; 2: retro-Michael addition;
DOI:10.1016/j.tet.2007.01.068

Reference yield:

: 934808-03-4
4-((S)-2-allyl-piperidin-1-yl)-N-benzyl-N-(2-cyanoethyl)-4-oxo-butyramide

: 934807-99-5
dec-9-enoic acid (3-{[4-(2-allyl-piperidin-1-yl)-butyl]-benzyl-amino}-propyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminum hydride / 25 °C

2: 276 mg / triethylamine / CH₂Cl₂ / 2 h / 0 °C

With lithium aluminium tetrahydride; triethylamine; In dichloromethane; 1: retro-Michael addition;
DOI:10.1016/j.tet.2007.01.068