N-(4-iodobenzyl)-1,2,3,4-tetrahydroquinaldine

Base Information

Chemical Name:N-(4-iodobenzyl)-1,2,3,4-tetrahydroquinaldine
CAS No.:1479311-36-8
Molecular Formula:C₁₆H₁₆IN
Molecular Weight:349.214
Hs Code.:

Synonyms:N-(4-iodobenzyl)-1,2,3,4-tetrahydroquinaldine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-iodobenzyl)-1,2,3,4-tetrahydroquinaldine

Chemical Property:

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Technology Process of N-(4-iodobenzyl)-1,2,3,4-tetrahydroquinaldine

There total 4 articles about N-(4-iodobenzyl)-1,2,3,4-tetrahydroquinaldine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 91-63-4
2-methylquinoline

: 15164-44-0
p-(iodophenyl)carboxaldehyde

: 18282-51-4
4-iodo-benzyl alcohol

: 1479311-36-8
N-(4-iodobenzyl)-1,2,3,4-tetrahydroquinaldine

: 1780-19-4
1,2,3,4-tetrahydro-2-methylquinoline

Guidance literature:: With (7,8-benzoquinolinato)hydrido(aqua)bis(triphenylphosphine)iridium(III) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen; In toluene; at 80 ℃; for 18h;
DOI:10.1021/om400267n

Reference yield:

: 91-63-4
2-methylquinoline

: 1479311-36-8
N-(4-iodobenzyl)-1,2,3,4-tetrahydroquinaldine

Guidance literature:: Multi-step reaction with 3 steps

1: (7,8-benzoquinolinato)hydrido(aqua)bis(triphenylphosphine)iridium(III) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen / toluene / 18 h / 20 °C / 760.05 Torr

2: potassium acetate / water; acetic acid / 18 h / 40 °C

3: sodium iodide / tetrahydrofuran / 24 h

With (7,8-benzoquinolinato)hydrido(aqua)bis(triphenylphosphine)iridium(III) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen; potassium acetate; sodium iodide; In tetrahydrofuran; water; acetic acid; toluene;
DOI:10.1021/om400267n