2,4-dihloro-5-fluorophenylglyoxal

Base Information

• Chemical Name: 2,4-dihloro-5-fluorophenylglyoxal
• CAS No.: 875119-43-0
• Molecular Formula: C₈H₃Cl₂FO₂
• Molecular Weight: 221.015

Synonyms:2,4-dihloro-5-fluorophenylglyoxal

Chemical Property of 2,4-dihloro-5-fluorophenylglyoxal

Chemical Property:

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Technology Process of 2,4-dihloro-5-fluorophenylglyoxal

There total 1 articles about 2,4-dihloro-5-fluorophenylglyoxal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2,4-dichloro-5-fluoroacetophenone (704-10-9) → 2,4-dihloro-5-fluorophenylglyoxal (875119-43-0)

Guidance literature:

With selenium(IV) oxide; silica gel; for 0.133333h; microwave irradiation;

Reference yield: 95.0%

2,4-dihloro-5-fluorophenylglyoxal (875119-43-0) + 2,4-DNP thio urea → 5-(2,4-dichloro-5-fluoro-phenyl)-1-(2,4-dinitro-phenyl)-2-thioxo-imidazolidin-4-one

Guidance literature:

With aluminum oxide; for 0.15h; microwave irradiation;

Reference yield: 95.0%

2,4-dihloro-5-fluorophenylglyoxal (875119-43-0) + p-tolylurea (622-51-5) → 5-(2,4-dichloro-5-fluoro-phenyl)-1-p-tolyl-imidazolidine-2,4-dione

Guidance literature:

With aluminum oxide; for 0.166667h; microwave irradiation;

upstream raw materials:

2,4-dichloro-5-fluoroacetophenone

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