3-(2'-Methylencyclohexyl)propylbromid

Base Information

• Chemical Name: 3-(2'-Methylencyclohexyl)propylbromid
• CAS No.: 52890-25-2
• Molecular Formula: C₁₀H₁₇Br
• Molecular Weight: 217.149
• Mol file: 52890-25-2.mol

Synonyms:3-(2'-Methylencyclohexyl)propylbromid

Chemical Property of 3-(2'-Methylencyclohexyl)propylbromid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(2'-Methylencyclohexyl)propylbromid

There total 7 articles about 3-(2'-Methylencyclohexyl)propylbromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Nitro-benzenesulfonic acid 3-(2-methylene-cyclohexyl)-propyl ester (52890-20-7) → 3-(2'-Methylencyclohexyl)propylbromid (52890-25-2)

Guidance literature:

With Pyridine hydrobromide; In N,N-dimethyl-formamide;

Reference yield:

1-(1-Cyclohexen-1-yl)pyrrolidine (1125-99-1) → 3-(2'-Methylencyclohexyl)propylbromid (52890-25-2)

Guidance literature:

Multi-step reaction with 5 steps

1: (i) EtOH, (ii) aq. AcOH

2: (i) NaH, DMSO, (ii) /BRN= 392747/

3: LiAlH₄ / diethyl ether

4: Py

5: Py*HBr / dimethylformamide

With pyridine; lithium aluminium tetrahydride; Pyridine hydrobromide; In diethyl ether; N,N-dimethyl-formamide;

Reference yield:

2-(3-hydroxypropyl)methylenecyclohexane (52890-23-0) → 3-(2'-Methylencyclohexyl)propylbromid (52890-25-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Py

2: Py*HBr / dimethylformamide

With pyridine; Pyridine hydrobromide; In N,N-dimethyl-formamide;

upstream raw materials:

4-Nitro-benzenesulfonic acid 3-(2-methylene-cyclohexyl)-propyl ester

2-(3'-bromopropyl)cyklohexanone

Methylenetriphenylphosphorane

ethyl 2-oxocyclohexane carboxylate

Downstream raw materials:

cis-hydrindane

decalin

2-n-propyl-1-methylenecyclohexane