phenyl 2-O-benzoyl-3-O-benzyl-6-O-(dimethylthexysilyl)-1-thio-α-L-idopyranoside

Base Information

• Chemical Name: phenyl 2-O-benzoyl-3-O-benzyl-6-O-(dimethylthexysilyl)-1-thio-α-L-idopyranoside
• CAS No.: 1447801-64-0
• Molecular Formula: C₃₉H₅₀O₈SSi
• Molecular Weight: 706.973

Synonyms:phenyl 2-O-benzoyl-3-O-benzyl-6-O-(dimethylthexysilyl)-1-thio-α-L-idopyranoside

Chemical Property of phenyl 2-O-benzoyl-3-O-benzyl-6-O-(dimethylthexysilyl)-1-thio-α-L-idopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl 2-O-benzoyl-3-O-benzyl-6-O-(dimethylthexysilyl)-1-thio-α-L-idopyranoside

There total 4 articles about phenyl 2-O-benzoyl-3-O-benzyl-6-O-(dimethylthexysilyl)-1-thio-α-L-idopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

phenyl 2-O-benzoyl-3-O-benzyl-6-O-(dimethylthexysilyl)-1-thio-α-L-idopyranoside (1447801-77-5) + levulinic acid (123-76-2) → phenyl 2-O-benzoyl-3-O-benzyl-6-O-(dimethylthexysilyl)-1-thio-α-L-idopyranoside (1447801-64-0)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 5h;

DOI:10.1021/jo400467g

Reference yield:

C21H22O6 → phenyl 2-O-benzoyl-3-O-benzyl-6-O-(dimethylthexysilyl)-1-thio-α-L-idopyranoside (1447801-64-0)

Guidance literature:

Multi-step reaction with 3 steps

1: zinc(II) iodide / dichloromethane / 20 °C

2: dmap; pyridine / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 5 h / 20 °C

With pyridine; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; zinc(II) iodide; In dichloromethane;

DOI:10.1021/jo400467g

Reference yield:

phenylthiotrimethylsilane (4551-15-9) → phenyl 2-O-benzoyl-3-O-benzyl-6-O-(dimethylthexysilyl)-1-thio-α-L-idopyranoside (1447801-64-0)

Guidance literature:

Multi-step reaction with 3 steps

1: zinc(II) iodide / dichloromethane / 20 °C

2: dmap; pyridine / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 5 h / 20 °C

With pyridine; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; zinc(II) iodide; In dichloromethane;

DOI:10.1021/jo400467g

upstream raw materials:

phenylthiotrimethylsilane

phenyl 2-O-benzoyl-3-O-benzyl-6-O-(dimethylthexysilyl)-1-thio-α-L-idopyranoside

levulinic acid

phenyl 2-O-benzoyl-3-O-benzyl-4,6-dihydroxylthio-α-L-idopyranoside

Downstream raw materials:

4-(hydroxymethyl)-benzyl N-benzyl-N-[5-((4-O-(2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3-O-benzyl-6-O-(dimethylthexylsilyl)-α-L-idopyranosyl)-oxy)pentyl]carbamate

2-O-benzoyl-3-O-benzyl-6-O-(dimethylthexylsilyl)-4-O-levulinoyl-α-L-idopyranosyl trichloroacetimidate

2-O-benzoyl-3-O-benzyl-6-O-(dimethylthexylsilyl)-4-O-levulinoyl-β-L-idopyranosyl trichloroacetimidate

4-(phenylcarboxymethyl)benzyl N-benzyl N-(5-(2-O-benzoyl-3-O-benzyl-6-O-dimethylthexylsilyl-α-L-idopyranosyloxy)pentyl) carbamate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1447801-64-0 phenyl 2-O-benzoyl-3-O-benzyl-6-O-(dimethylthexysilyl)-1-thio-α-L-idopyranoside

Send

Send

Metric Ton KG G Pound L ML

Send

Send