cyclopropyl-(7,8-dimethoxy-1-phenyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)methanone

Base Information

Chemical Name:cyclopropyl-(7,8-dimethoxy-1-phenyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)methanone
CAS No.:1201682-01-0
Molecular Formula:C₂₂H₂₅NO₃
Molecular Weight:351.445
Hs Code.:

Synonyms:cyclopropyl-(7,8-dimethoxy-1-phenyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)methanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclopropyl-(7,8-dimethoxy-1-phenyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)methanone

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Technology Process of cyclopropyl-(7,8-dimethoxy-1-phenyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)methanone

There total 1 articles about cyclopropyl-(7,8-dimethoxy-1-phenyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 20569-49-7
7,8-dimethoxy-1-phenyl-2,3,4,5-tetrahydro-1H-3-benzazepine

: 4023-34-1
cyclopropanecarboxylic acid chloride

: 1201682-01-0
cyclopropyl-(7,8-dimethoxy-1-phenyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)methanone

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/chem.200901197

Reference yield:

: 1201682-01-0
cyclopropyl-(7,8-dimethoxy-1-phenyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)methanone

: 1268628-08-5
C₂₂H₂₃NO₃⁽¹⁸⁾O

Guidance literature:: With iron(III) chloride; oxygen; ¹⁸O-labeled water; In nitrobenzene; at 120 ℃;
DOI:10.1016/j.tet.2010.12.038

Reference yield:

: 1201682-01-0
cyclopropyl-(7,8-dimethoxy-1-phenyl-4,5-dihydro-1H-benzo[d]azepin-3(2H)-yl)methanone

: 1201682-08-7
2-(cyclopropanecarbonyl)-6,7-dimethoxy-1-phenyl-1,2,3,4-tetrahydroisoquinoline-1-carbaldehyde

: 1268627-80-0
(4-chloro-7,8-dimethoxy-5-phenyl-1H-benzo[d]azepin-3(2H)-yl)(cyclopropyl)methanone

Guidance literature:: With iron(III) chloride hexahydrate; water; oxygen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In nitromethane; for 4h; Reflux;
DOI:10.1016/j.tet.2010.12.038