4b,6a-dihydro-5-phenylcyclobutaphenanthrene

Base Information

• Chemical Name: 4b,6a-dihydro-5-phenylcyclobutaphenanthrene
• CAS No.: 158059-35-9
• Molecular Formula: C₂₂H₁₆
• Molecular Weight: 280.369
• Mol file: 158059-35-9.mol

Synonyms:4b,6a-dihydro-5-phenylcyclobutaphenanthrene

Chemical Property of 4b,6a-dihydro-5-phenylcyclobutaphenanthrene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4b,6a-dihydro-5-phenylcyclobutaphenanthrene

There total 3 articles about 4b,6a-dihydro-5-phenylcyclobutaphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

6-phenyldibenzocyclooctene → 4b,6a-dihydro-5-phenylcyclobutaphenanthrene (158059-35-9)

Guidance literature:

In benzene; at 10 ℃; for 2h; Irradiation;

DOI:10.1002/hlca.19940770324

Reference yield:

phenylmagnesium bromide (100-58-3) → 4b,6a-dihydro-5-phenylcyclobutaphenanthrene (158059-35-9)

Guidance literature:

Multi-step reaction with 2 steps

2: 67 percent / benzene / 2 h / 10 °C / Irradiation

In benzene;

DOI:10.1002/hlca.19940770324

Reference yield:

5,6-dihydrodibenzocycloocten-6-one → 4b,6a-dihydro-5-phenylcyclobutaphenanthrene (158059-35-9)

Guidance literature:

Multi-step reaction with 2 steps

2: 67 percent / benzene / 2 h / 10 °C / Irradiation

In benzene;

DOI:10.1002/hlca.19940770324

upstream raw materials:

phenylmagnesium bromide