Benzoic acid (3S,5R,8R,9S,10R,13R,14R,15S,17R)-17-((R)-1,5-dimethyl-hexyl)-4,4,10,13-tetramethyl-hexadecahydro-20-oxa-cyclopropa[14,15]cyclopenta[a]phenanthren-3-yl ester

Base Information

Chemical Name:Benzoic acid (3S,5R,8R,9S,10R,13R,14R,15S,17R)-17-((R)-1,5-dimethyl-hexyl)-4,4,10,13-tetramethyl-hexadecahydro-20-oxa-cyclopropa[14,15]cyclopenta[a]phenanthren-3-yl ester
CAS No.:309958-28-9
Molecular Formula:C₃₆H₅₄O₃
Molecular Weight:534.823
Hs Code.:

Benzoic acid (3S,5R,8R,9S,10R,13R,14R,15S,17R)-17-((R)-1,5-dimethyl-hexyl)-4,4,10,13-tetramethyl-hexadecahydro-20-oxa-cyclopropa[14,15]cyclopenta[a]phenanthren-3-yl ester

Synonyms:Benzoic acid (3S,5R,8R,9S,10R,13R,14R,15S,17R)-17-((R)-1,5-dimethyl-hexyl)-4,4,10,13-tetramethyl-hexadecahydro-20-oxa-cyclopropa[14,15]cyclopenta[a]phenanthren-3-yl ester

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Chemical Property of Benzoic acid (3S,5R,8R,9S,10R,13R,14R,15S,17R)-17-((R)-1,5-dimethyl-hexyl)-4,4,10,13-tetramethyl-hexadecahydro-20-oxa-cyclopropa[14,15]cyclopenta[a]phenanthren-3-yl ester

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Technology Process of Benzoic acid (3S,5R,8R,9S,10R,13R,14R,15S,17R)-17-((R)-1,5-dimethyl-hexyl)-4,4,10,13-tetramethyl-hexadecahydro-20-oxa-cyclopropa[14,15]cyclopenta[a]phenanthren-3-yl ester

There total 6 articles about Benzoic acid (3S,5R,8R,9S,10R,13R,14R,15S,17R)-17-((R)-1,5-dimethyl-hexyl)-4,4,10,13-tetramethyl-hexadecahydro-20-oxa-cyclopropa[14,15]cyclopenta[a]phenanthren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 309958-27-8
Benzoic acid (3S,5R,8R,9S,10R,13R,17R)-17-((R)-1,5-dimethyl-hexyl)-4,4,10,13-tetramethyl-2,3,4,5,6,7,8,9,10,11,12,13,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

: 309958-28-9
Benzoic acid (3S,5R,8R,9S,10R,13R,14R,15S,17R)-17-((R)-1,5-dimethyl-hexyl)-4,4,10,13-tetramethyl-hexadecahydro-20-oxa-cyclopropa[14,15]cyclopenta[a]phenanthren-3-yl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 53296-71-2
(3β,20R)-4,4-dimethylcholesta-5,7-dien-3-ol

: 309958-28-9
Benzoic acid (3S,5R,8R,9S,10R,13R,14R,15S,17R)-17-((R)-1,5-dimethyl-hexyl)-4,4,10,13-tetramethyl-hexadecahydro-20-oxa-cyclopropa[14,15]cyclopenta[a]phenanthren-3-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10 percent Pd/C / ethyl acetate

2: pyridine

3: 70 percent / HCl gas / CH₂Cl₂ / 0.5 h / -20 °C

4: 64 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 0 °C

With pyridine; hydrogenchloride; hydrogen; 3-chloro-benzenecarboperoxoic acid; 10% palladium on active carbon; In dichloromethane; ethyl acetate;

Reference yield:

: 7638-67-7
32-nor-lanosta-5,7-dien-3-one

: 309958-28-9
Benzoic acid (3S,5R,8R,9S,10R,13R,14R,15S,17R)-17-((R)-1,5-dimethyl-hexyl)-4,4,10,13-tetramethyl-hexadecahydro-20-oxa-cyclopropa[14,15]cyclopenta[a]phenanthren-3-yl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 63 percent / LiAlH₄ / tetrahydrofuran / 1.5 h

2: H₂ / 10 percent Pd/C / ethyl acetate

3: pyridine

4: 70 percent / HCl gas / CH₂Cl₂ / 0.5 h / -20 °C

5: 64 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 0 °C

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; hydrogen; 3-chloro-benzenecarboperoxoic acid; 10% palladium on active carbon; In tetrahydrofuran; dichloromethane; ethyl acetate;