(S)-2-{2-[2-((S)-1,2-Dicarbamoyl-ethylcarbamoyl)-phenyldisulfanyl]-benzoylamino}-succinamide

Base Information

Chemical Name:(S)-2-{2-[2-((S)-1,2-Dicarbamoyl-ethylcarbamoyl)-phenyldisulfanyl]-benzoylamino}-succinamide
CAS No.:219310-03-9
Molecular Formula:C₂₂H₂₄N₆O₆S₂
Molecular Weight:532.601
Hs Code.:

Synonyms:(S)-2-{2-[2-((S)-1,2-Dicarbamoyl-ethylcarbamoyl)-phenyldisulfanyl]-benzoylamino}-succinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-{2-[2-((S)-1,2-Dicarbamoyl-ethylcarbamoyl)-phenyldisulfanyl]-benzoylamino}-succinamide

Chemical Property:

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Technology Process of (S)-2-{2-[2-((S)-1,2-Dicarbamoyl-ethylcarbamoyl)-phenyldisulfanyl]-benzoylamino}-succinamide

There total 2 articles about (S)-2-{2-[2-((S)-1,2-Dicarbamoyl-ethylcarbamoyl)-phenyldisulfanyl]-benzoylamino}-succinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 19602-82-5
2,2'-dithiodibenzoic acid dichloride

: 57471-69-9
L-asparaginamide hydrochloride

: 219310-03-9
(S)-2-{2-[2-((S)-1,2-Dicarbamoyl-ethylcarbamoyl)-phenyldisulfanyl]-benzoylamino}-succinamide

Guidance literature:: With 4-methyl-morpholine; In N,N-dimethyl acetamide; at 20 ℃;
DOI:10.1016/S0968-0896(01)00392-3

Reference yield:

: 119-80-2
2,2'-dithiobenzoic acid

: 219310-03-9
(S)-2-{2-[2-((S)-1,2-Dicarbamoyl-ethylcarbamoyl)-phenyldisulfanyl]-benzoylamino}-succinamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 80 °C

2: 78 percent / 4-methylmorpholine / N,N-dimethyl-acetamide / 20 °C

With 4-methyl-morpholine; thionyl chloride; In N,N-dimethyl acetamide;
DOI:10.1016/S0968-0896(01)00392-3

Reference yield:

: 219310-03-9
(S)-2-{2-[2-((S)-1,2-Dicarbamoyl-ethylcarbamoyl)-phenyldisulfanyl]-benzoylamino}-succinamide

: (S)-2-(2-Mercapto-benzoylamino)-succinamide

Guidance literature:: With tris(carboxyethyl)phosphine hydrochloride; triethylamine; In water; N,N-dimethyl-formamide; at 25 ℃;
DOI:10.1016/S0968-0896(01)00392-3