ethyl (+/-)-3-phenyl-4-[4-[3-(1-oxopyridin-2-yl)amino-1-propyloxy]phenyl]butanoate

Base Information

Chemical Name:ethyl (+/-)-3-phenyl-4-[4-[3-(1-oxopyridin-2-yl)amino-1-propyloxy]phenyl]butanoate
CAS No.:243641-76-1
Molecular Formula:C₂₆H₃₀N₂O₄
Molecular Weight:434.535
Hs Code.:

Synonyms:ethyl (+/-)-3-phenyl-4-[4-[3-(1-oxopyridin-2-yl)amino-1-propyloxy]phenyl]butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (+/-)-3-phenyl-4-[4-[3-(1-oxopyridin-2-yl)amino-1-propyloxy]phenyl]butanoate

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Technology Process of ethyl (+/-)-3-phenyl-4-[4-[3-(1-oxopyridin-2-yl)amino-1-propyloxy]phenyl]butanoate

There total 4 articles about ethyl (+/-)-3-phenyl-4-[4-[3-(1-oxopyridin-2-yl)amino-1-propyloxy]phenyl]butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 187339-14-6
2-(3-hydroxypropyl)aminopyridine-N-oxide

: 193533-32-3
ethyl (+/-)-4-(4-hydroxyphenyl)-3-phenylbutanoate

: 243641-76-1
ethyl (+/-)-3-phenyl-4-[4-[3-(1-oxopyridin-2-yl)amino-1-propyloxy]phenyl]butanoate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(03)00102-1

Reference yield: 51.0%

: 187339-14-6
2-(3-hydroxypropyl)aminopyridine-N-oxide

: 243642-49-1
ethyl (R)-(+)-4-(4-hydroxyphenyl)-3-phenylbutanoate

: 243641-76-1
ethyl (+/-)-3-phenyl-4-[4-[3-(1-oxopyridin-2-yl)amino-1-propyloxy]phenyl]butanoate

Guidance literature:: With diisopropyl (E)-azodicarboxylate; triphenylphosphine; In N,N-dimethyl-formamide;

Reference yield:

: 24845-40-7
2-(4-methoxyphenyl)acetophenone

: 243641-76-1
ethyl (+/-)-3-phenyl-4-[4-[3-(1-oxopyridin-2-yl)amino-1-propyloxy]phenyl]butanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 96 percent / LiN(TMS)2 / tetrahydrofuran

2.1: Et₃Si; BF₃*OEt₂ / CH₂Cl₂

2.2: 91 percent / H₂ / 10 percent Pd/C / ethanol

3.1: 96 percent / EtSH; AlCl₃ / CH₂Cl₂

4.1: 68 percent / DIAD; (Ph₃)P / dimethylformamide

With triethylsilane; aluminium trichloride; di-isopropyl azodicarboxylate; boron trifluoride diethyl etherate; triphenylphosphine; ethanethiol; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(03)00102-1