5-O-acetyl-3-azido-1-O-(4-biphenylcarbonyl)-2,3-dideoxy-D-erythro-pentofuranose

Base Information

Chemical Name:5-O-acetyl-3-azido-1-O-(4-biphenylcarbonyl)-2,3-dideoxy-D-erythro-pentofuranose
CAS No.:135281-02-6
Molecular Formula:C₂₀H₁₉N₃O₅
Molecular Weight:381.388
Hs Code.:

Synonyms:5-O-acetyl-3-azido-1-O-(4-biphenylcarbonyl)-2,3-dideoxy-D-erythro-pentofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-O-acetyl-3-azido-1-O-(4-biphenylcarbonyl)-2,3-dideoxy-D-erythro-pentofuranose

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Technology Process of 5-O-acetyl-3-azido-1-O-(4-biphenylcarbonyl)-2,3-dideoxy-D-erythro-pentofuranose

There total 3 articles about 5-O-acetyl-3-azido-1-O-(4-biphenylcarbonyl)-2,3-dideoxy-D-erythro-pentofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122359-33-5
(+)-(2E,4S)-5-Acetoxy-4-(formyloxy)-2-pentenal

: 135281-02-6
5-O-acetyl-3-azido-1-O-(4-biphenylcarbonyl)-2,3-dideoxy-D-erythro-pentofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / NaHCO₃ / methanol / 0.75 h / Ambient temperature

2: 80 percent AcOH / 24 h / Ambient temperature

3: pyridine / CH₂Cl₂ / 1) 0 deg C, 1 h 2) r.t. 20 h

With pyridine; sodium hydrogencarbonate; acetic acid; In methanol; dichloromethane;
DOI:10.1055/s-1991-26490

Reference yield:

: 135357-51-6
(2E,4S)-5-acetoxy-4-hydroxy-2-pentenal

: 135281-02-6
5-O-acetyl-3-azido-1-O-(4-biphenylcarbonyl)-2,3-dideoxy-D-erythro-pentofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent AcOH / 24 h / Ambient temperature

2: pyridine / CH₂Cl₂ / 1) 0 deg C, 1 h 2) r.t. 20 h

With pyridine; acetic acid; In dichloromethane;
DOI:10.1055/s-1991-26490

Reference yield:

: 14002-51-8
4-biphenyl-carboxylic acid chloride

: Acetic acid (S)-3-azido-5-hydroxy-tetrahydro-furan-2-ylmethyl ester

: 135281-03-7
5-O-acetyl-3-azido-1-O-(4-biphenylcarbonyl)-2,3-dideoxy-D-threo-pentofuranose

: 135281-02-6
5-O-acetyl-3-azido-1-O-(4-biphenylcarbonyl)-2,3-dideoxy-D-erythro-pentofuranose

Guidance literature:: With pyridine; In dichloromethane; Yield given. Yields of byproduct given; 1) 0 deg C, 1 h 2) r.t. 20 h;
DOI:10.1055/s-1991-26490