S-phenyl [(7-(hex-5-en-1-yl)-1,4-dioxaspiro[4.5]dec-8-en-7-yl)methyl](4-methoxybenzyl)carbamothioate

Base Information

Chemical Name:S-phenyl [(7-(hex-5-en-1-yl)-1,4-dioxaspiro[4.5]dec-8-en-7-yl)methyl](4-methoxybenzyl)carbamothioate
CAS No.:1440419-50-0
Molecular Formula:C₃₀H₃₇NO₄S
Molecular Weight:507.694
Hs Code.:

Synonyms:S-phenyl [(7-(hex-5-en-1-yl)-1,4-dioxaspiro[4.5]dec-8-en-7-yl)methyl](4-methoxybenzyl)carbamothioate

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Chemical Property of S-phenyl [(7-(hex-5-en-1-yl)-1,4-dioxaspiro[4.5]dec-8-en-7-yl)methyl](4-methoxybenzyl)carbamothioate

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Technology Process of S-phenyl [(7-(hex-5-en-1-yl)-1,4-dioxaspiro[4.5]dec-8-en-7-yl)methyl](4-methoxybenzyl)carbamothioate

There total 10 articles about S-phenyl [(7-(hex-5-en-1-yl)-1,4-dioxaspiro[4.5]dec-8-en-7-yl)methyl](4-methoxybenzyl)carbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 39594-84-8
4-methylphenyl chlorothioformate

: 1440419-49-7
N-{[7-(hex-5-en-1-yl)-1,4-dioxaspiro[4.5]dec-8-en-7-yl]methyl}-1-(4-methoxyphenyl)methanamine

: 1440419-50-0
S-phenyl [(7-(hex-5-en-1-yl)-1,4-dioxaspiro[4.5]dec-8-en-7-yl)methyl](4-methoxybenzyl)carbamothioate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1002/cjoc.202000291

Reference yield: 95.0%

: 13464-19-2
phenyl chlorothioformate

: 1440419-49-7
N-{[7-(hex-5-en-1-yl)-1,4-dioxaspiro[4.5]dec-8-en-7-yl]methyl}-1-(4-methoxyphenyl)methanamine

: 1440419-50-0
S-phenyl [(7-(hex-5-en-1-yl)-1,4-dioxaspiro[4.5]dec-8-en-7-yl)methyl](4-methoxybenzyl)carbamothioate

Guidance literature:: N-{[7-(hex-5-en-1-yl)-1,4-dioxaspiro[4.5]dec-8-en-7-yl]methyl}-1-(4-methoxyphenyl)methanamine; With dmap; triethylamine; In dichloromethane; for 1h;

phenyl chlorothioformate; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/chem.201203203

Reference yield:

: 5323-87-5
3-Ethoxycyclohex-2-en-1-one

: 1440419-50-0
S-phenyl [(7-(hex-5-en-1-yl)-1,4-dioxaspiro[4.5]dec-8-en-7-yl)methyl](4-methoxybenzyl)carbamothioate

Guidance literature:: Multi-step reaction with 7 steps

1.1: diethyl ether; tetrahydrofuran / 12 h / 0 - 20 °C

2.1: rac-Pro-OH; 2,5-dimethyl-piperazine / chloroform / 168 h / 50 °C

3.1: 2-iodoxybenzoic acid; 4-methylmorpholine N-oxide / dimethyl sulfoxide / 72 h / 20 - 45 °C

4.1: toluene-4-sulfonic acid / toluene / 24 h / Dean-Stark; Inert atmosphere; Reflux

5.1: lithium aluminium tetrahydride / diethyl ether / 6 h / 0 - 20 °C

6.1: sodium tris(acetoxy)borohydride / dichloromethane / 5 h / 20 °C

7.1: dmap; triethylamine / dichloromethane / 1 h

7.2: 0 - 20 °C

With dmap; lithium aluminium tetrahydride; 2-iodoxybenzoic acid; sodium tris(acetoxy)borohydride; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triethylamine; 2,5-dimethyl-piperazine; rac-Pro-OH; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform; dimethyl sulfoxide; toluene;
DOI:10.1002/chem.201203203