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Technology Process of [(H)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))](CH2)6[(CH3)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))]

[(H)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))](CH2)6[(CH3)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))]

Base Information
  • Chemical Name:[(H)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))](CH2)6[(CH3)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))]
  • CAS No.:157442-89-2
  • Molecular Formula:C113H106N8O2Rh2
  • Molecular Weight:1813.95
  • Hs Code.:
[(H)Rh(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)3(C<sub>6</sub>H<sub>4</sub>O))](CH<sub>2</sub>)6[(CH<sub>3</sub>)Rh(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)3(C<sub>6</sub>H<sub>4</sub>O))]

Synonyms:[(H)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))](CH2)6[(CH3)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))]

Suppliers and Price of [(H)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))](CH2)6[(CH3)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))]
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Chemical Property of [(H)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))](CH2)6[(CH3)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))]
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Technology Process of [(H)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))](CH2)6[(CH3)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))]

There total 2 articles about [(H)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))](CH2)6[(CH3)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[Rh(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)3(C<sub>6</sub>H<sub>4</sub>))O]2(CH<sub>2</sub>)6
157442-88-1

[Rh(C20H8N4(C6H2(CH3)3)3(C6H4))O]2(CH2)6

[(H)Rh(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)3(C<sub>6</sub>H<sub>4</sub>O))](CH<sub>2</sub>)6[(CH<sub>3</sub>)Rh(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)3(C<sub>6</sub>H<sub>4</sub>O))]
157442-89-2

[(H)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))](CH2)6[(CH3)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))]

Guidance literature:
With methane; In benzene-d6; react. of Rh-complex with CH4 (pressure = 1.0 atm) at 296 K in C6D6; not isolated, detected by 1H-NMR spect.; Kinetics;
DOI:10.1021/ja00096a057

Reference yield:

methane
34557-54-5,27936-85-2

methane

[Rh(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)3(C<sub>6</sub>H<sub>4</sub>))O]2(CH<sub>2</sub>)6
157442-88-1

[Rh(C20H8N4(C6H2(CH3)3)3(C6H4))O]2(CH2)6

carbon monoxide
201230-82-2

carbon monoxide

[(H)Rh(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)3(C<sub>6</sub>H<sub>4</sub>O))](CH<sub>2</sub>)6[(CH<sub>3</sub>)Rh(C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)3(C<sub>6</sub>H<sub>4</sub>O))]
157442-89-2

[(H)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))](CH2)6[(CH3)Rh(C20H8N4(C6H2(CH3)3)3(C6H4O))]

Guidance literature:
In benzene; inert atm.; 0.37 atm CO, then 0.53 atm CH4;
DOI:10.1021/ja962248n
upstream raw materials:

[Rh(C20H8N4(C6H2(CH3)3)3(C6H4))O]2(CH2)6

methane

carbon monoxide

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