Technology Process of ethyl 6-O-benzyl-2-O-(4-methoxybenzyl)-thio-β-D-galactopyran-3,4-diol
There total 7 articles about ethyl 6-O-benzyl-2-O-(4-methoxybenzyl)-thio-β-D-galactopyran-3,4-diol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
water; acetic acid;
at 50 ℃;
Inert atmosphere;
DOI:10.1021/ml300263x
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: water; acetic acid / 50 °C / Inert atmosphere
With
sodium hydride;
In
water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/ml300263x
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / Inert atmosphere
2.1: hydrogenchloride / 1,4-dioxane / Inert atmosphere; Reflux
3.1: pyridine; dmap / Inert atmosphere
4.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / Inert atmosphere
5.1: sodium methylate / methanol / Inert atmosphere
6.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / Inert atmosphere
7.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere
7.2: 20 °C / Inert atmosphere
8.1: water; acetic acid / 50 °C / Inert atmosphere
With
pyridine; hydrogenchloride; dmap; trimethylsilyl trifluoromethanesulfonate; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid;
In
1,4-dioxane; methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/ml300263x
