(E)-3-{(2S,3R)-1-[(R)-2,2-Bis-propylsulfanyl-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-3-methoxy-4-oxo-azetidin-2-yl}-acrylic acid benzhydryl ester

Base Information

Chemical Name:(E)-3-{(2S,3R)-1-[(R)-2,2-Bis-propylsulfanyl-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-3-methoxy-4-oxo-azetidin-2-yl}-acrylic acid benzhydryl ester
CAS No.:162398-36-9
Molecular Formula:C₃₈H₅₁NO₈S₂
Molecular Weight:713.957
Hs Code.:

(E)-3-{(2S,3R)-1-[(R)-2,2-Bis-propylsulfanyl-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-3-methoxy-4-oxo-azetidin-2-yl}-acrylic acid benzhydryl ester

Synonyms:(E)-3-{(2S,3R)-1-[(R)-2,2-Bis-propylsulfanyl-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-3-methoxy-4-oxo-azetidin-2-yl}-acrylic acid benzhydryl ester

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Chemical Property of (E)-3-{(2S,3R)-1-[(R)-2,2-Bis-propylsulfanyl-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-3-methoxy-4-oxo-azetidin-2-yl}-acrylic acid benzhydryl ester

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Technology Process of (E)-3-{(2S,3R)-1-[(R)-2,2-Bis-propylsulfanyl-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-3-methoxy-4-oxo-azetidin-2-yl}-acrylic acid benzhydryl ester

There total 3 articles about (E)-3-{(2S,3R)-1-[(R)-2,2-Bis-propylsulfanyl-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-3-methoxy-4-oxo-azetidin-2-yl}-acrylic acid benzhydryl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88726-02-7
4-oxobuten-⁽²⁾-oic acid benzhydryl ester

: 162398-36-9
(E)-3-{(2S,3R)-1-[(R)-2,2-Bis-propylsulfanyl-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-3-methoxy-4-oxo-azetidin-2-yl}-acrylic acid benzhydryl ester

Guidance literature:: Multi-step reaction with 2 steps

2: Et₃N / toluene / Ambient temperature

With triethylamine; In toluene;
DOI:10.1016/S0957-4166(00)86289-8

Reference yield:

: sorbic acid benzhydryl ester

: 162398-36-9
(E)-3-{(2S,3R)-1-[(R)-2,2-Bis-propylsulfanyl-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-3-methoxy-4-oxo-azetidin-2-yl}-acrylic acid benzhydryl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) O₃, 2.) Me₂S / 1.) CH₂Cl₂, -60 deg C, 2.) CH₂Cl₂, 20 deg C

3: Et₃N / toluene / Ambient temperature

With dimethylsulfide; ozone; triethylamine; In toluene;
DOI:10.1016/S0957-4166(00)86289-8

Reference yield:

: 38870-89-2
Methoxyacetyl chloride

: 162398-33-6
(E)-4-[(Z)-(R)-2,2-Bis-propylsulfanyl-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethylimino]-but-2-enoic acid benzhydryl ester

: 162490-37-1
(E)-3-{(2R,3S)-1-[(R)-2,2-Bis-propylsulfanyl-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-3-methoxy-4-oxo-azetidin-2-yl}-acrylic acid benzhydryl ester

: 162398-36-9
(E)-3-{(2S,3R)-1-[(R)-2,2-Bis-propylsulfanyl-1-((4S,5R,4'R)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]-5-yl)-ethyl]-3-methoxy-4-oxo-azetidin-2-yl}-acrylic acid benzhydryl ester

Guidance literature:: With triethylamine; In toluene; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1016/S0957-4166(00)86289-8