dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-hydroxymethyl-2-nitro-propyl] ester O-ethyl ester

Base Information

Chemical Name:dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-hydroxymethyl-2-nitro-propyl] ester O-ethyl ester
CAS No.:588706-88-1
Molecular Formula:C₂₈H₂₈N₂O₆S₂
Molecular Weight:552.672
Hs Code.:

dithiocarbonic acid <i>S</i>-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-hydroxymethyl-2-nitro-propyl] ester <i>O</i>-ethyl ester

Synonyms:dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-hydroxymethyl-2-nitro-propyl] ester O-ethyl ester

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Chemical Property of dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-hydroxymethyl-2-nitro-propyl] ester O-ethyl ester

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Technology Process of dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-hydroxymethyl-2-nitro-propyl] ester O-ethyl ester

There total 4 articles about dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-hydroxymethyl-2-nitro-propyl] ester O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 588706-83-6
dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-nitro-propyl] ester O-ethyl ester

: 588706-88-1
dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-hydroxymethyl-2-nitro-propyl] ester O-ethyl ester

Guidance literature:: With potassium ethyl xanthogenate; In tetrahydrofuran; water; acetic acid; for 120h;
DOI:10.1021/ol035027c

Reference yield:

: 21473-46-1
2-(4'-benzyloxy-3'-methoxyphenyl)-1-nitroethane

: 588706-88-1
dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-hydroxymethyl-2-nitro-propyl] ester O-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / acetic acid; n-butylamine / toluene / 4 h / Heating

2: 80 percent / acetic acid / 0 - 20 °C

3: 40 percent / potassium O-ethyl xanthate / H₂O; tetrahydrofuran; acetic acid / 120 h

With potassium ethyl xanthogenate; acetic acid; N-butylamine; In tetrahydrofuran; water; acetic acid; toluene; 1: Knoevenagel reaction / 2: Michael addition;
DOI:10.1021/ol035027c

Reference yield:

: 105-07-7
4-cyanobenzaldehyde

: 588706-88-1
dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-(4-cyano-phenyl)-2-hydroxymethyl-2-nitro-propyl] ester O-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / acetic acid; n-butylamine / toluene / 4 h / Heating

2: 80 percent / acetic acid / 0 - 20 °C

3: 40 percent / potassium O-ethyl xanthate / H₂O; tetrahydrofuran; acetic acid / 120 h

With potassium ethyl xanthogenate; acetic acid; N-butylamine; In tetrahydrofuran; water; acetic acid; toluene; 1: Knoevenagel reaction / 2: Michael addition;
DOI:10.1021/ol035027c