3-(((E)-2-(3-nitrobenzoyl)hydrazono)methyl)-4-phenyl-1,2,5-oxadiazole 2-oxide

Base Information

Chemical Name:3-(((E)-2-(3-nitrobenzoyl)hydrazono)methyl)-4-phenyl-1,2,5-oxadiazole 2-oxide
CAS No.:1617522-33-4
Molecular Formula:C₁₆H₁₁N₅O₅
Molecular Weight:353.294
Hs Code.:

Synonyms:3-(((E)-2-(3-nitrobenzoyl)hydrazono)methyl)-4-phenyl-1,2,5-oxadiazole 2-oxide

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Chemical Property of 3-(((E)-2-(3-nitrobenzoyl)hydrazono)methyl)-4-phenyl-1,2,5-oxadiazole 2-oxide

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Technology Process of 3-(((E)-2-(3-nitrobenzoyl)hydrazono)methyl)-4-phenyl-1,2,5-oxadiazole 2-oxide

There total 3 articles about 3-(((E)-2-(3-nitrobenzoyl)hydrazono)methyl)-4-phenyl-1,2,5-oxadiazole 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 135733-34-5
4-phenylfuroxan-3-carboxaldehyde

: 618-94-0
3-nitrobenzoic acid hydrazide

: 1617522-33-4
3-(((E)-2-(3-nitrobenzoyl)hydrazono)methyl)-4-phenyl-1,2,5-oxadiazole 2-oxide

: 1617522-67-4
3-(((Z)-2-(3-nitrobenzoyl)hydrazono)methyl)-4-phenyl-1,2,5-oxadiazole 2-oxide

Guidance literature:: With hydrogenchloride; In ethanol; Overall yield = 63 %; Reflux;
DOI:10.1016/j.ejmech.2014.05.077

Reference yield:

: 121-92-6
3-nitrobenzoic acid

: 1617522-33-4
3-(((E)-2-(3-nitrobenzoyl)hydrazono)methyl)-4-phenyl-1,2,5-oxadiazole 2-oxide

: 1617522-67-4
3-(((Z)-2-(3-nitrobenzoyl)hydrazono)methyl)-4-phenyl-1,2,5-oxadiazole 2-oxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / ethanol; water / Reflux

1.2: 4 h / 60 °C

2.1: hydrogenchloride / ethanol / Reflux

With hydrogenchloride; sulfuric acid; In ethanol; water;
DOI:10.1016/j.ejmech.2014.05.077

Reference yield:

: 104-54-1
3-Phenylpropenol

: 1617522-33-4
3-(((E)-2-(3-nitrobenzoyl)hydrazono)methyl)-4-phenyl-1,2,5-oxadiazole 2-oxide

: 1617522-67-4
3-(((Z)-2-(3-nitrobenzoyl)hydrazono)methyl)-4-phenyl-1,2,5-oxadiazole 2-oxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; acetic acid / water / 1 h / 70 °C

1.2: 5 h / 20 °C

2.1: hydrogenchloride / ethanol / Reflux

With hydrogenchloride; acetic acid; sodium nitrite; In ethanol; water;
DOI:10.1016/j.ejmech.2014.05.077