5-{3'-methyl-5'-acetyl-4'-(4-nitrophenyl)-pyrazolo{3',4'-c}pyrazol-1-yl-sulfonyl}-8-quinolinol

Base Information

Chemical Name:5-{3'-methyl-5'-acetyl-4'-(4-nitrophenyl)-pyrazolo{3',4'-c}pyrazol-1-yl-sulfonyl}-8-quinolinol
CAS No.:145800-10-8
Molecular Formula:C₂₂H₁₈N₆O₆S
Molecular Weight:494.488
Hs Code.:

Synonyms:5-{3'-methyl-5'-acetyl-4'-(4-nitrophenyl)-pyrazolo{3',4'-c}pyrazol-1-yl-sulfonyl}-8-quinolinol

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Chemical Property of 5-{3'-methyl-5'-acetyl-4'-(4-nitrophenyl)-pyrazolo{3',4'-c}pyrazol-1-yl-sulfonyl}-8-quinolinol

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Technology Process of 5-{3'-methyl-5'-acetyl-4'-(4-nitrophenyl)-pyrazolo{3',4'-c}pyrazol-1-yl-sulfonyl}-8-quinolinol

There total 3 articles about 5-{3'-methyl-5'-acetyl-4'-(4-nitrophenyl)-pyrazolo{3',4'-c}pyrazol-1-yl-sulfonyl}-8-quinolinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 64-19-7,77671-22-8
acetic acid

: 144101-60-0
2-(8-Hydroxy-quinoline-5-sulfonyl)-5-methyl-4-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-2,4-dihydro-pyrazol-3-one

: 145800-10-8
5-{3'-methyl-5'-acetyl-4'-(4-nitrophenyl)-pyrazolo{3',4'-c}pyrazol-1-yl-sulfonyl}-8-quinolinol

Guidance literature:: With hydrazine hydrate; for 8h; Heating;

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 145800-10-8
5-{3'-methyl-5'-acetyl-4'-(4-nitrophenyl)-pyrazolo{3',4'-c}pyrazol-1-yl-sulfonyl}-8-quinolinol

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Et₃N / ethanol / 1 h / Heating

2: 50 percent / NH₂-NH₂*H₂O / 8 h / Heating

With hydrazine hydrate; triethylamine; In ethanol;

Reference yield:

: 136950-28-2
5-<3'-methyl-5'-oxo-4',5'-dihydropyrazol-1-yl-sulfonyl>-8-quinolinol

: 145800-10-8
5-{3'-methyl-5'-acetyl-4'-(4-nitrophenyl)-pyrazolo{3',4'-c}pyrazol-1-yl-sulfonyl}-8-quinolinol

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Et₃N / ethanol / 1 h / Heating

2: 50 percent / NH₂-NH₂*H₂O / 8 h / Heating

With hydrazine hydrate; triethylamine; In ethanol;