(R)-benzyl (1-chloropent-4-en-2-yl)oxycarbamate

Base Information

Chemical Name:(R)-benzyl (1-chloropent-4-en-2-yl)oxycarbamate
CAS No.:1613376-35-4
Molecular Formula:C₁₃H₁₆ClNO₃
Molecular Weight:269.728
Hs Code.:

Synonyms:(R)-benzyl (1-chloropent-4-en-2-yl)oxycarbamate

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Chemical Property of (R)-benzyl (1-chloropent-4-en-2-yl)oxycarbamate

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Technology Process of (R)-benzyl (1-chloropent-4-en-2-yl)oxycarbamate

There total 3 articles about (R)-benzyl (1-chloropent-4-en-2-yl)oxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1613376-34-3
(R)-O-(1-chloropent-4-en-2-yl)hydroxylamine

: 501-53-1,94274-21-2
benzyl chloroformate

: 1613376-35-4
(R)-benzyl (1-chloropent-4-en-2-yl)oxycarbamate

Guidance literature:: With sodium carbonate; In dichloromethane; water; at 0 - 20 ℃; for 3h;
DOI:10.1039/c4ob00537f

Reference yield:

: 953047-22-8
(2S)-1-chloropent-4-en-2-ol

: 1613376-35-4
(R)-benzyl (1-chloropent-4-en-2-yl)oxycarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

2: hydrazine hydrate / dichloromethane / 0.25 h / 0 - 20 °C

3: sodium carbonate / dichloromethane; water / 3 h / 0 - 20 °C

With di-isopropyl azodicarboxylate; sodium carbonate; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; 1: |Mitsunobu Displacement;
DOI:10.1039/c4ob00537f

Reference yield:

: 1613376-33-2
(R)-2-(1-chloropent-4-en-2-yloxy)isoindoline-1,3-dione

: 1613376-35-4
(R)-benzyl (1-chloropent-4-en-2-yl)oxycarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / dichloromethane / 0.25 h / 0 - 20 °C

2: sodium carbonate / dichloromethane; water / 3 h / 0 - 20 °C

With sodium carbonate; hydrazine hydrate; In dichloromethane; water;
DOI:10.1039/c4ob00537f