4-cyano-N-{2,6-dichloro-4-[1-(4-chlorophenyl)-1,2,2,2-tetrafluoroethyl]phenyl}-3-nitrobenzamide

Base Information

Chemical Name:4-cyano-N-{2,6-dichloro-4-[1-(4-chlorophenyl)-1,2,2,2-tetrafluoroethyl]phenyl}-3-nitrobenzamide
CAS No.:1321562-68-8
Molecular Formula:C₂₂H₁₀Cl₃F₄N₃O₃
Molecular Weight:546.692
Hs Code.:

Synonyms:4-cyano-N-{2,6-dichloro-4-[1-(4-chlorophenyl)-1,2,2,2-tetrafluoroethyl]phenyl}-3-nitrobenzamide

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Chemical Property of 4-cyano-N-{2,6-dichloro-4-[1-(4-chlorophenyl)-1,2,2,2-tetrafluoroethyl]phenyl}-3-nitrobenzamide

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Technology Process of 4-cyano-N-{2,6-dichloro-4-[1-(4-chlorophenyl)-1,2,2,2-tetrafluoroethyl]phenyl}-3-nitrobenzamide

There total 3 articles about 4-cyano-N-{2,6-dichloro-4-[1-(4-chlorophenyl)-1,2,2,2-tetrafluoroethyl]phenyl}-3-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1321562-65-5
2,6-dichloro-4-[1-(4-chlorophenyl)-1,2,2,2-tetrafluoroethyl]-phenylamine

: 153775-42-9
2-nitro-4-carboxybenzonitrile

: 1321562-68-8
4-cyano-N-{2,6-dichloro-4-[1-(4-chlorophenyl)-1,2,2,2-tetrafluoroethyl]phenyl}-3-nitrobenzamide

Guidance literature:: With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In 1,2-dichloro-ethane; at 110 ℃;

Reference yield:

: 23516-79-2
4-(trifluoroacetyl)aniline

: 1321562-68-8
4-cyano-N-{2,6-dichloro-4-[1-(4-chlorophenyl)-1,2,2,2-tetrafluoroethyl]phenyl}-3-nitrobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: N-chloro-succinimide / acetonitrile / 1.5 h / Reflux

2: tetrahydrofuran / 0 °C / Inert atmosphere

3: (bis-(2-methoxyethyl)amino)sulfur trufluoride / tetrahydrofuran / 2 h / 0 °C

4: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / 1,2-dichloro-ethane / 110 °C

With N-chloro-succinimide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran; 1,2-dichloro-ethane; acetonitrile;

Reference yield:

: 1321562-47-3
1-(4-amino-3,5-dichlorophenyl)-2,2,2-trifluoroethanone

: 1321562-68-8
4-cyano-N-{2,6-dichloro-4-[1-(4-chlorophenyl)-1,2,2,2-tetrafluoroethyl]phenyl}-3-nitrobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 0 °C / Inert atmosphere

2: (bis-(2-methoxyethyl)amino)sulfur trufluoride / tetrahydrofuran / 2 h / 0 °C

3: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / 1,2-dichloro-ethane / 110 °C

With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran; 1,2-dichloro-ethane;