N(P(C₆H₅)3)2⁽¹⁺⁾*Mo(NCS)(CO)5^(1-)=[N(P(C₆H₅)3)2][Mo(NCS)(CO)5]

Base Information

Chemical Name:N(P(C₆H₅)3)2⁽¹⁺⁾*Mo(NCS)(CO)5^(1-)=[N(P(C₆H₅)3)2][Mo(NCS)(CO)5]
CAS No.:39048-40-3
Molecular Formula:C₆MoNO₅S*C₃₆H₃₀NP₂
Molecular Weight:832.664
Hs Code.:

N(P(C<sub>6</sub>H<sub>5</sub>)3)2<sup>(1+)</sup>*Mo(NCS)(CO)5<sup>(1-)</sup>=[N(P(C<sub>6</sub>H<sub>5</sub>)3)2][Mo(NCS)(CO)5]

Synonyms:N(P(C₆H₅)3)2⁽¹⁺⁾*Mo(NCS)(CO)5^(1-)=[N(P(C₆H₅)3)2][Mo(NCS)(CO)5]

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Chemical Property of N(P(C₆H₅)3)2⁽¹⁺⁾*Mo(NCS)(CO)5^(1-)=[N(P(C₆H₅)3)2][Mo(NCS)(CO)5]

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Technology Process of N(P(C₆H₅)3)2⁽¹⁺⁾*Mo(NCS)(CO)5^(1-)=[N(P(C₆H₅)3)2][Mo(NCS)(CO)5]

There total 1 articles about N(P(C₆H₅)3)2⁽¹⁺⁾*Mo(NCS)(CO)5^(1-)=[N(P(C₆H₅)3)2][Mo(NCS)(CO)5] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 21050-13-5
bis(triphenylphosphine)iminium chloride

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 39048-40-3
N(P(C₆H₅)3)2⁽¹⁺⁾*Mo(NCS)(CO)5^(1-)=[N(P(C₆H₅)3)2][Mo(NCS)(CO)5]

Guidance literature:: With KSCN; In dichloromethane; diethylene glycol dimethyl ether; N2-atmosphere; refluxing slight excess of Mo(CO)6 with KSCN for 10 min (in diglyme), cooling, addn. of stoich. amt. of PPNCl (in CH2Cl2), stirring for 1 h; pptn. on addn. of light petroleum, decantation, washing, chromy. (Al2O3,CH2Cl2), evapn.;
DOI:10.1039/DT9780001255

Reference yield:

: 421-20-5
Methyl fluorosulfonate

: 39048-40-3
N(P(C₆H₅)3)2⁽¹⁺⁾*Mo(NCS)(CO)5^(1-)=[N(P(C₆H₅)3)2][Mo(NCS)(CO)5]

: 69073-95-6
Mo(CO)5(NCSCH₃)

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

Guidance literature:: In dichloromethane; N2-atmosphere, room temp.; excess FSO2OMe, stirring for 0.5 h; solvent removal (reduced pressure), extn. into hexane; product mixt. notsepd., detd. by IR spectroscopy;
DOI:10.1039/DT9780001255