2-(Benzylidenamino)-3-(dimethylamino)-2-methylpropansaeure-methylester-N-oxid

Base Information

Chemical Name:2-(Benzylidenamino)-3-(dimethylamino)-2-methylpropansaeure-methylester-N-oxid
CAS No.:79751-23-8
Molecular Formula:C₁₄H₂₀N₂O₃
Molecular Weight:264.324
Hs Code.:

Synonyms:2-(Benzylidenamino)-3-(dimethylamino)-2-methylpropansaeure-methylester-N-oxid

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Chemical Property of 2-(Benzylidenamino)-3-(dimethylamino)-2-methylpropansaeure-methylester-N-oxid

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Technology Process of 2-(Benzylidenamino)-3-(dimethylamino)-2-methylpropansaeure-methylester-N-oxid

There total 3 articles about 2-(Benzylidenamino)-3-(dimethylamino)-2-methylpropansaeure-methylester-N-oxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 622-32-2
(Z)-benzaldehyde oxime

: 79751-23-8
2-(Benzylidenamino)-3-(dimethylamino)-2-methylpropansaeure-methylester-N-oxid

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / NaOMe / methanol

2: 1) tert-BuOK / 1) THF, -70 deg C, 30 min, 2) THF, room temperature

3: 1) LDA / 1) THF, -40 deg C, 30 min, 2) THF, room temperature

With potassium tert-butylate; sodium methylate; lithium diisopropyl amide; In methanol;

Reference yield:

: 79751-42-1
(Benzylidenamino)ethansaeure-methylester-N-oxid

: 79751-23-8
2-(Benzylidenamino)-3-(dimethylamino)-2-methylpropansaeure-methylester-N-oxid

Guidance literature:: Multi-step reaction with 2 steps

1: 1) tert-BuOK / 1) THF, -70 deg C, 30 min, 2) THF, room temperature

2: 1) LDA / 1) THF, -40 deg C, 30 min, 2) THF, room temperature

With potassium tert-butylate; lithium diisopropyl amide;

Reference yield:

: 58581-44-5
2-(Benzylidenamino)propansaeure-methylester-N-oxid

: 30354-18-8
N,N-dimethyl(methylene)ammonium chloride

: 79751-23-8
2-(Benzylidenamino)-3-(dimethylamino)-2-methylpropansaeure-methylester-N-oxid

: 79751-24-9
2-(Benzylidenamino)-3-(diisopropylamino)-2-methylpropansaeure-methylester-N-oxid

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given; 1) THF, -40 deg C, 30 min, 2) THF, room temperature;