C₂₉H₃₁NO₃S

Base Information

Chemical Name:C₂₉H₃₁NO₃S
CAS No.:1446655-34-0
Molecular Formula:C₂₉H₃₁NO₃S
Molecular Weight:473.636
Hs Code.:

C<sub>29</sub>H<sub>31</sub>NO<sub>3</sub>S

Synonyms:C₂₉H₃₁NO₃S

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Chemical Property of C₂₉H₃₁NO₃S

Chemical Property:

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Technology Process of C₂₉H₃₁NO₃S

There total 11 articles about C₂₉H₃₁NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 4410-99-5
2-mercaptophenylethane

: 1446655-40-8
C₂₂H₂₅NO₆S

: 1446655-34-0
C₂₉H₃₁NO₃S

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃;

Reference yield:

: 51-35-4,30724-02-8
4R-4-hydroxyproline

: 1446655-34-0
C₂₉H₃₁NO₃S

Guidance literature:: Multi-step reaction with 11 steps

1.1: thionyl chloride / Reflux

2.1: potassium carbonate / water; diethyl ether / 2 h / 0 - 20 °C

3.1: triethylamine / dichloromethane / 20 - 40 °C

4.1: cesium fluoride / N,N-dimethyl-formamide / 40 h / 60 °C

5.1: 1 h / 0 - 20 °C

5.2: 48 h / 20 °C

6.1: sodium hydroxide / tetrahydrofuran / 1.5 h / 0 - 20 °C

6.2: pH 3 - 4

7.1: borane-THF / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

8.1: palladium 10% on activated carbon; hydrogen / methanol / 760.05 Torr

9.1: potassium hydrogencarbonate / 0.5 h / 0 °C

10.1: triethylamine / dichloromethane / 0.5 h / 0 °C

11.1: caesium carbonate / N,N-dimethyl-formamide / 80 °C

With thionyl chloride; borane-THF; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydrogencarbonate; caesium carbonate; triethylamine; cesium fluoride; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 33996-30-4
trans-4-hydroxy-L-proline ethyl ester hydrochloride

: 1446655-34-0
C₂₉H₃₁NO₃S

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate / water; diethyl ether / 2 h / 0 - 20 °C

2.1: triethylamine / dichloromethane / 20 - 40 °C

3.1: cesium fluoride / N,N-dimethyl-formamide / 40 h / 60 °C

4.1: 1 h / 0 - 20 °C

4.2: 48 h / 20 °C

5.1: sodium hydroxide / tetrahydrofuran / 1.5 h / 0 - 20 °C

5.2: pH 3 - 4

6.1: borane-THF / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

7.1: palladium 10% on activated carbon; hydrogen / methanol / 760.05 Torr

8.1: potassium hydrogencarbonate / 0.5 h / 0 °C

9.1: triethylamine / dichloromethane / 0.5 h / 0 °C

10.1: caesium carbonate / N,N-dimethyl-formamide / 80 °C

With borane-THF; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydrogencarbonate; caesium carbonate; triethylamine; cesium fluoride; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;