4-methyl-3-(4-methylpiperazin-1-yl)-5-(2-(methylsulfonamido)ethoxy)-2-oxo-2H-chromen-7-yl 4-methylbenzenesulfonate

Base Information

Chemical Name:4-methyl-3-(4-methylpiperazin-1-yl)-5-(2-(methylsulfonamido)ethoxy)-2-oxo-2H-chromen-7-yl 4-methylbenzenesulfonate
CAS No.:1456808-62-0
Molecular Formula:C₂₅H₃₁N₃O₈S₂
Molecular Weight:565.668
Hs Code.:

Synonyms:4-methyl-3-(4-methylpiperazin-1-yl)-5-(2-(methylsulfonamido)ethoxy)-2-oxo-2H-chromen-7-yl 4-methylbenzenesulfonate

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Chemical Property of 4-methyl-3-(4-methylpiperazin-1-yl)-5-(2-(methylsulfonamido)ethoxy)-2-oxo-2H-chromen-7-yl 4-methylbenzenesulfonate

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Technology Process of 4-methyl-3-(4-methylpiperazin-1-yl)-5-(2-(methylsulfonamido)ethoxy)-2-oxo-2H-chromen-7-yl 4-methylbenzenesulfonate

There total 8 articles about 4-methyl-3-(4-methylpiperazin-1-yl)-5-(2-(methylsulfonamido)ethoxy)-2-oxo-2H-chromen-7-yl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1456808-55-1
5-(2-aminoethoxy)-4-methyl-3-(4-methylpiperazin-1-yl)-2-oxo-2H-chromen-7-yl 4-methylbenzenesulfonate

: 124-63-0
methanesulfonyl chloride

: 1456808-62-0
4-methyl-3-(4-methylpiperazin-1-yl)-5-(2-(methylsulfonamido)ethoxy)-2-oxo-2H-chromen-7-yl 4-methylbenzenesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.ejmech.2013.04.015

Reference yield:

: 1456807-82-1
C₂₉H₃₀N₂O₈S₂

: 1456808-62-0
4-methyl-3-(4-methylpiperazin-1-yl)-5-(2-(methylsulfonamido)ethoxy)-2-oxo-2H-chromen-7-yl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 °C

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0.33 h / 20 °C

3: acetic acid / dichloromethane / 1 h / 40 °C

4: triethylamine / dichloromethane / 20 °C

With tetrabutyl ammonium fluoride; acetic acid; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 2: |Mitsunobu Displacement;
DOI:10.1016/j.ejmech.2013.04.015

Reference yield:

: 1456807-88-7
C₂₂H₂₄N₂O₆S

: 1456808-62-0
4-methyl-3-(4-methylpiperazin-1-yl)-5-(2-(methylsulfonamido)ethoxy)-2-oxo-2H-chromen-7-yl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0.33 h / 20 °C

2: acetic acid / dichloromethane / 1 h / 40 °C

3: triethylamine / dichloromethane / 20 °C

With acetic acid; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 1: |Mitsunobu Displacement;
DOI:10.1016/j.ejmech.2013.04.015