(1,3-Dioxo-1,3-dihydro-isoindol-2-yloxymethyl)-phenyl-phosphinic acid isopropyl ester

Base Information

Chemical Name:(1,3-Dioxo-1,3-dihydro-isoindol-2-yloxymethyl)-phenyl-phosphinic acid isopropyl ester
CAS No.:145433-36-9
Molecular Formula:C₁₈H₁₈NO₅P
Molecular Weight:359.318
Hs Code.:

Synonyms:(1,3-Dioxo-1,3-dihydro-isoindol-2-yloxymethyl)-phenyl-phosphinic acid isopropyl ester

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Chemical Property of (1,3-Dioxo-1,3-dihydro-isoindol-2-yloxymethyl)-phenyl-phosphinic acid isopropyl ester

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Technology Process of (1,3-Dioxo-1,3-dihydro-isoindol-2-yloxymethyl)-phenyl-phosphinic acid isopropyl ester

There total 2 articles about (1,3-Dioxo-1,3-dihydro-isoindol-2-yloxymethyl)-phenyl-phosphinic acid isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 524-38-9
N-hydroxyphthalimide

: 145433-29-0
i-propyl hydroxymethane(phenyl)phosphinate

: 145433-36-9
(1,3-Dioxo-1,3-dihydro-isoindol-2-yloxymethyl)-phenyl-phosphinic acid isopropyl ester

Guidance literature:: With diethyl azodicarbonate; triphenylphosphine; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 81261-25-8
Hydroxy-isopropyloxy-phenyl-phosphin

: 145433-36-9
(1,3-Dioxo-1,3-dihydro-isoindol-2-yloxymethyl)-phenyl-phosphinic acid isopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 67.1 percent / Et₃N / 120 °C

2: 100 percent / triphenylphosphine, azodicarbonic acid diethyl ester / tetrahydrofuran / 20 °C

With diethyl azodicarbonate; triphenylphosphine; triethylamine; In tetrahydrofuran;