3,4,6-tri-O-acetyl-1,2-O-<1-ethylidene>-α-D-glucopyranose

Base Information

Chemical Name:3,4,6-tri-O-acetyl-1,2-O-<1-ethylidene>-α-D-glucopyranose
CAS No.:98911-13-8
Molecular Formula:C₂₈H₂₈Cl₃NO₁₂
Molecular Weight:676.889
Hs Code.:

3,4,6-tri-O-acetyl-1,2-O-<1-<N-acetyl-4-(2,4,6-trichlorophenoxy)-anilino-oxy>ethylidene>-α-D-glucopyranose

Synonyms:3,4,6-tri-O-acetyl-1,2-O-<1-ethylidene>-α-D-glucopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4,6-tri-O-acetyl-1,2-O-<1-ethylidene>-α-D-glucopyranose

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Technology Process of 3,4,6-tri-O-acetyl-1,2-O-<1-ethylidene>-α-D-glucopyranose

There total 2 articles about 3,4,6-tri-O-acetyl-1,2-O-<1-ethylidene>-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 98911-09-2
2,4,6-Trichloro-4'-hydroxyacetylaminobiphenyl ether

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 98911-13-8
3,4,6-tri-O-acetyl-1,2-O-<1-ethylidene>-α-D-glucopyranose

Guidance literature:: With 2,6-dimethylpyridine; In nitromethane; at 37 ℃; for 42h; in the dark;

Reference yield:

: 1836-77-7
p-nitrophenyl 2,4,6-trichlorophenyl ether

: 98911-13-8
3,4,6-tri-O-acetyl-1,2-O-<1-ethylidene>-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) aq. ammonium chloride, zinc 2.) sodium hydrogen carbonate / 1.) dioxane, 15 min 2.) ether, water, 1.5 h

2: 84 percent / 2,6-lutidine / nitromethane / 42 h / 37 °C / in the dark

With 2,6-dimethylpyridine; ammonium chloride; sodium hydrogencarbonate; zinc; In nitromethane;