C₄₄H₅₀N₂O₈

Base Information

• Chemical Name: C₄₄H₅₀N₂O₈
• CAS No.: 1185756-58-4
• Molecular Formula: C₄₄H₅₀N₂O₈
• Molecular Weight: 734.89
• Mol file: 1185756-58-4.mol

Synonyms:C₄₄H₅₀N₂O₈

Chemical Property of C₄₄H₅₀N₂O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of C₄₄H₅₀N₂O₈

There total 1 articles about C₄₄H₅₀N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-iodomethyl-3,5-dimethylphenyl ethyl carbonate (1185756-57-3) + 1,4-N,N-[(S)-1-phenylethyl]-piperazine-2,5-dione (158547-56-9) → C44H50N2O8 (1185756-58-4)

Guidance literature:

1,4-N,N-[(S)-1-phenylethyl]-piperazine-2,5-dione; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

4-iodomethyl-3,5-dimethylphenyl ethyl carbonate; In tetrahydrofuran; diastereoselective reaction; Further stages; Inert atmosphere;

DOI:10.1016/j.tetasy.2009.06.004

Reference yield: 100.0%

C44H50N2O8 (1185756-58-4) → H-Dmt (123715-02-6)

Guidance literature:

With hydrogen iodide; for 3h; Reflux;

DOI:10.1016/j.tetasy.2009.06.004

upstream raw materials:

4-iodomethyl-3,5-dimethylphenyl ethyl carbonate

1,4-N,N-[(S)-1-phenylethyl]-piperazine-2,5-dione

Downstream raw materials:

H-Dmt