(Z)-2,2-dimethyl-1,3-propanediyl α-acetyl-2-(trifluoromethyl)styrylphosphonate

Base Information

Chemical Name:(Z)-2,2-dimethyl-1,3-propanediyl α-acetyl-2-(trifluoromethyl)styrylphosphonate
CAS No.:115599-90-1
Molecular Formula:C₁₆H₁₈F₃O₄P
Molecular Weight:362.285
Hs Code.:

Synonyms:(Z)-2,2-dimethyl-1,3-propanediyl α-acetyl-2-(trifluoromethyl)styrylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2,2-dimethyl-1,3-propanediyl α-acetyl-2-(trifluoromethyl)styrylphosphonate

Chemical Property:

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Technology Process of (Z)-2,2-dimethyl-1,3-propanediyl α-acetyl-2-(trifluoromethyl)styrylphosphonate

There total 6 articles about (Z)-2,2-dimethyl-1,3-propanediyl α-acetyl-2-(trifluoromethyl)styrylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 1.0%

: 111011-80-4
2-acetonyl-5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinane

: 152401-80-4
2-(dimorpholinomethyl)-1-(trifluoromethyl)benzene

: 447-61-0
2-Trifluoromethylbenzaldehyde

: 115599-90-1
(Z)-2,2-dimethyl-1,3-propanediyl α-acetyl-2-(trifluoromethyl)styrylphosphonate

: 115578-88-6
(E)-2,2-dimethyl-1,3-propanediyl α-acetyl-2-(trifluoromethyl)styrylphosphonate

Guidance literature:: With chloroacetic acid; In toluene; for 3h; Yield given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1055/s-1993-25926

Reference yield: 1.0%

: 111011-80-4
2-acetonyl-5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinane

: 152401-80-4
2-(dimorpholinomethyl)-1-(trifluoromethyl)benzene

: 447-61-0
2-Trifluoromethylbenzaldehyde

: 115599-90-1
(Z)-2,2-dimethyl-1,3-propanediyl α-acetyl-2-(trifluoromethyl)styrylphosphonate

: 115578-88-6
(E)-2,2-dimethyl-1,3-propanediyl α-acetyl-2-(trifluoromethyl)styrylphosphonate

: 2,2-dimethyl-1,3-propanediyl 2-oxo-4-<2-(trifluoromethyl)phenyl>-3-butenylphosphonate

Guidance literature:: With trifluoroacetic acid; Yield given. Multistep reaction. Title compound not separated from byproducts; 1) toluene, 2) r.t., 3.0 h;
DOI:10.1055/s-1993-25926

Reference yield:

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 115599-90-1
(Z)-2,2-dimethyl-1,3-propanediyl α-acetyl-2-(trifluoromethyl)styrylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: phosphorus trichloride / diethyl ether; CH₂Cl₂ / 2 h / Ambient temperature

2: triethylamine / diethyl ether / 2 h / Ambient temperature

3: 51 percent / 1 h / 80 °C

4: piperidine*AcOH / benzene / Heating

With triethylamine; phosphorus trichloride; piperdinium acetate; In diethyl ether; dichloromethane; benzene;
DOI:10.1248/cpb.35.4144