4-chloro-N,N-diethyl-α-oxo-benzeneacetamide

Base Information

Chemical Name:4-chloro-N,N-diethyl-α-oxo-benzeneacetamide
CAS No.:84039-66-7
Molecular Formula:C₁₂H₁₄ClNO₂
Molecular Weight:239.702
Hs Code.:

Synonyms:4-chloro-N,N-diethyl-α-oxo-benzeneacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-N,N-diethyl-α-oxo-benzeneacetamide

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Technology Process of 4-chloro-N,N-diethyl-α-oxo-benzeneacetamide

There total 13 articles about 4-chloro-N,N-diethyl-α-oxo-benzeneacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 873-73-4
4-n-chlorophenylacetylene

: 61582-64-7
N,N-diethyl-O-benzoylhydroxylamine

: 84039-66-7
4-chloro-N,N-diethyl-α-oxo-benzeneacetamide

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c6ra15219h

Reference yield: 80.0%

: 617-84-5
N-formyldiethylamine

: 99-91-2
para-chloroacetophenone

: 84039-66-7
4-chloro-N,N-diethyl-α-oxo-benzeneacetamide

Guidance literature:: With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; In water; at 100 ℃; for 16h;
DOI:10.1039/c2cc35279f

Reference yield: 77.0%

: 7099-88-9
4-chlorophenylglyoxylic acid

: 121-44-8
triethylamine

: 84039-66-7
4-chloro-N,N-diethyl-α-oxo-benzeneacetamide

Guidance literature:: With silver (II) carbonate; dipotassium peroxodisulfate; In tetrachloromethane; N,N-dimethyl-formamide; at 120 ℃; for 12h;
DOI:10.1039/c3ob40619a