Technology Process of C2HF3O2*C16H23N5O3
There total 6 articles about C2HF3O2*C16H23N5O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride; benzotriazol-1-ol; 1,2-dichloro-ethane; triethylamine / dichloromethane / 20 °C
2: dichloromethane
With
hydrogenchloride; benzotriazol-1-ol; 1,2-dichloro-ethane; triethylamine;
In
dichloromethane;
DOI:10.1073/pnas.1015267108
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium azide; trifluoromethylsulfonic anhydride; potassium carbonate; copper(II) sulfate / methanol; dichloromethane; water / 0 - 20 °C
2: hydrogenchloride; benzotriazol-1-ol; 1,2-dichloro-ethane; triethylamine / dichloromethane / 20 °C
3: dichloromethane
With
hydrogenchloride; sodium azide; trifluoromethylsulfonic anhydride; potassium carbonate; benzotriazol-1-ol; copper(II) sulfate; 1,2-dichloro-ethane; triethylamine;
In
methanol; dichloromethane; water;
DOI:10.1073/pnas.1015267108
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride; dmap; 1,2-dichloro-ethane
2: palladium on activated charcoal; hydrogen / methanol
3: hydrogenchloride; benzotriazol-1-ol; 1,2-dichloro-ethane; triethylamine / dichloromethane / 20 °C
4: dichloromethane
With
hydrogenchloride; dmap; palladium on activated charcoal; hydrogen; benzotriazol-1-ol; 1,2-dichloro-ethane; triethylamine;
In
methanol; dichloromethane;
DOI:10.1073/pnas.1015267108