C₃₆H₅₄N₄O₇

Base Information

Chemical Name:C₃₆H₅₄N₄O₇
CAS No.:1271773-39-7
Molecular Formula:C₃₆H₅₄N₄O₇
Molecular Weight:654.847
Hs Code.:

C<sub>36</sub>H<sub>54</sub>N<sub>4</sub>O<sub>7</sub>

Synonyms:C₃₆H₅₄N₄O₇

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Chemical Property of C₃₆H₅₄N₄O₇

Chemical Property:

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Technology Process of C₃₆H₅₄N₄O₇

There total 10 articles about C₃₆H₅₄N₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1271773-36-4
C₂₁H₃₅N₃O₃

: 62023-65-8
(2S,3R)-3-[(tert-butoxycarbonyl) amino]-2-hydroxy-4-phenyl-butanoic acid

: 1271773-39-7
C₃₆H₅₄N₄O₇

Guidance literature:: (2S,3R)-3-[(tert-butoxycarbonyl) amino]-2-hydroxy-4-phenyl-butanoic acid; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 1h;

C₂₁H₃₅N₃O₃; In dichloromethane; at 0 - 20 ℃; for 18h;

Reference yield:

: 1271773-08-0
C₂₁H₂₁NO₃

: 1271773-39-7
C₃₆H₅₄N₄O₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / -78 - 20 °C

2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C

3.1: hydrazine hydrate / ethanol / 3 h / Heating; Reflux

4.1: sodium hydrogencarbonate / 1,4-dioxane; water / 5 h

5.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol; tetrahydrofuran / 16 h / 0 - 20 °C

6.1: sodium periodate / water; tetrahydrofuran / 3.5 h / 0 °C

7.1: pyridinium chlorochromate / dichloromethane / 20 °C / Molecular sieves 3?

8.1: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C

9.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C

9.2: 18 h / 0 - 20 °C

10.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C

10.2: 18 h / 0 - 20 °C

With sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; water; sodium hydrogencarbonate; benzotriazol-1-ol; hydrazine hydrate; 4-methylmorpholine N-oxide; dicyclohexyl-carbodiimide; triphenylphosphine; pyridinium chlorochromate; lithium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; tert-butyl alcohol;

Reference yield:

: 1271773-25-1
C₁₇H₂₇NO₄

: 1271773-39-7
C₃₆H₅₄N₄O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium periodate / water; tetrahydrofuran / 3.5 h / 0 °C

2.1: pyridinium chlorochromate / dichloromethane / 20 °C / Molecular sieves 3?

3.1: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C

4.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C

4.2: 18 h / 0 - 20 °C

5.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C

5.2: 18 h / 0 - 20 °C

With sodium periodate; water; benzotriazol-1-ol; dicyclohexyl-carbodiimide; pyridinium chlorochromate; lithium hydroxide; In tetrahydrofuran; dichloromethane; water;