(2S)-3-(3-benzyloxy-5,6,7,8-tetrahydro-2-naphthoxy)-1,2-bis(mesyloxy)propane

Base Information

Chemical Name:(2S)-3-(3-benzyloxy-5,6,7,8-tetrahydro-2-naphthoxy)-1,2-bis(mesyloxy)propane
CAS No.:753022-36-5
Molecular Formula:C₂₂H₂₈O₈S₂
Molecular Weight:484.592
Hs Code.:

Synonyms:(2S)-3-(3-benzyloxy-5,6,7,8-tetrahydro-2-naphthoxy)-1,2-bis(mesyloxy)propane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-3-(3-benzyloxy-5,6,7,8-tetrahydro-2-naphthoxy)-1,2-bis(mesyloxy)propane

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Technology Process of (2S)-3-(3-benzyloxy-5,6,7,8-tetrahydro-2-naphthoxy)-1,2-bis(mesyloxy)propane

There total 3 articles about (2S)-3-(3-benzyloxy-5,6,7,8-tetrahydro-2-naphthoxy)-1,2-bis(mesyloxy)propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 753022-35-4
(R)-3-(3-benzyloxy-5,6,7,8-tetrahydro-2-naphthoxy)-1,2-propanediol

: 124-63-0
methanesulfonyl chloride

: 753022-36-5
(2S)-3-(3-benzyloxy-5,6,7,8-tetrahydro-2-naphthoxy)-1,2-bis(mesyloxy)propane

Guidance literature:: With TEA; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2004.06.040

Reference yield:

: 753022-34-3
2-benzyloxy-3-acetoxy-5,6,7,8-tetrahydronaphthalene

: 753022-36-5
(2S)-3-(3-benzyloxy-5,6,7,8-tetrahydro-2-naphthoxy)-1,2-bis(mesyloxy)propane

Guidance literature:: Multi-step reaction with 3 steps

1.1: 29 g / NaOH / methanol; H₂O / 5 h / 20 °C

2.1: KOH / ethanol / 24 h / Heating

2.2: 59 percent / HCl / methanol; H₂O / 3 h / 75 °C

3.1: 87 percent / TEA / CH₂Cl₂ / 2 h / 20 °C

With potassium hydroxide; sodium hydroxide; TEA; In methanol; ethanol; dichloromethane; water;
DOI:10.1016/j.bmc.2004.06.040

Reference yield:

: 125101-78-2
3-benzyloxy-5,6,7,8-tetrahydro-2-naphthol

: 753022-36-5
(2S)-3-(3-benzyloxy-5,6,7,8-tetrahydro-2-naphthoxy)-1,2-bis(mesyloxy)propane

Guidance literature:: Multi-step reaction with 2 steps

1.1: KOH / ethanol / 24 h / Heating

1.2: 59 percent / HCl / methanol; H₂O / 3 h / 75 °C

2.1: 87 percent / TEA / CH₂Cl₂ / 2 h / 20 °C

With potassium hydroxide; TEA; In ethanol; dichloromethane;
DOI:10.1016/j.bmc.2004.06.040