(R)-2-benzyloxycarbonylamino-3-amino-1-methylaminopropane

Base Information

Chemical Name:(R)-2-benzyloxycarbonylamino-3-amino-1-methylaminopropane
CAS No.:167949-67-9
Molecular Formula:C₂₅H₃₅N₃O₄
Molecular Weight:441.571
Hs Code.:

(R)-2-benzyloxycarbonylamino-3-<N-tert-butoxycarbonyl-N-(3-methylbenzyl)>amino-1-methylaminopropane

Synonyms:(R)-2-benzyloxycarbonylamino-3-amino-1-methylaminopropane

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Chemical Property of (R)-2-benzyloxycarbonylamino-3-amino-1-methylaminopropane

Chemical Property:

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Technology Process of (R)-2-benzyloxycarbonylamino-3-amino-1-methylaminopropane

There total 7 articles about (R)-2-benzyloxycarbonylamino-3-amino-1-methylaminopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 167949-67-9
(R)-2-benzyloxycarbonylamino-3-amino-1-methylaminopropane

Guidance literature:: Multi-step reaction with 3 steps

1: 25 g / CHCl₃ / 2 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

3: ethanol / 6 h / Heating

With triethylamine; In ethanol; dichloromethane; chloroform;
DOI:10.1248/cpb.46.1160

Reference yield:

: 6081-61-4
N-(benzyloxycarbonyl)-D-serine

: 167949-67-9
(R)-2-benzyloxycarbonylamino-3-amino-1-methylaminopropane

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride / CHCl₃ / 16 h / Ambient temperature

2: 1.) BH₃*THF, 2.) 1N aq. HCl / 1.) THF, RT, 16 h, 2.) THF, reflux, 4 h

3: 25 g / CHCl₃ / 2 h / Ambient temperature

4: Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

5: ethanol / 6 h / Heating

With hydrogenchloride; borane-THF; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In ethanol; dichloromethane; chloroform;
DOI:10.1248/cpb.46.1160

Reference yield:

: 100-81-2
3-methyl-benzenemethanamine

: 167949-67-9
(R)-2-benzyloxycarbonylamino-3-amino-1-methylaminopropane

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride / CHCl₃ / 16 h / Ambient temperature

2: 1.) BH₃*THF, 2.) 1N aq. HCl / 1.) THF, RT, 16 h, 2.) THF, reflux, 4 h

3: 25 g / CHCl₃ / 2 h / Ambient temperature

4: Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

5: ethanol / 6 h / Heating

With hydrogenchloride; borane-THF; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In ethanol; dichloromethane; chloroform;
DOI:10.1248/cpb.46.1160