N-(4-butylphenyl)-3-(4-(2-isopropylphenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(4-butylphenyl)-3-(4-(2-isopropylphenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide
CAS No.:1311382-59-8
Molecular Formula:C₃₁H₃₉N₃O₃S
Molecular Weight:533.735
Hs Code.:

Synonyms:N-(4-butylphenyl)-3-(4-(2-isopropylphenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide

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Chemical Property of N-(4-butylphenyl)-3-(4-(2-isopropylphenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-(4-butylphenyl)-3-(4-(2-isopropylphenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide

There total 5 articles about N-(4-butylphenyl)-3-(4-(2-isopropylphenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 377769-51-2
5-(N-(4-butylphenyl)sulfamoyl)-2-methylbenzoic acid

: 119695-82-8
1-[2-(methylethyl)phenyl]piperazine

: 1311382-59-8
N-(4-butylphenyl)-3-(4-(2-isopropylphenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide

Guidance literature:: 5-(N-(4-butylphenyl)sulfamoyl)-2-methylbenzoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

1-[2-(methylethyl)phenyl]piperazine; In N,N-dimethyl-formamide; at 0 - 20 ℃;

Reference yield:

: 7073-94-1
1-bromo-2-isopropylbenzene

: 1311382-59-8
N-(4-butylphenyl)-3-(4-(2-isopropylphenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium t-butanolate / 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 100 °C / Inert atmosphere

2.1: hydrogenchloride / methanol / 2 h

3.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.25 h / 0 °C

3.2: 0 - 20 °C

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In methanol; N,N-dimethyl-formamide; toluene;

Reference yield:

: 89001-57-0
5-(chlorosulfonyl)-2-methylbenzenecarboxylic acid

: 1311382-59-8
N-(4-butylphenyl)-3-(4-(2-isopropylphenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.25 h / 0 °C

2.2: 0 - 20 °C

With pyridine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;